GCMS analysis results for sample AD30489, Jan 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\HPCHEM\1\DATA\DEC3101\30489.D Vial: 11 Acq On : 31 Dec 2001 8:42 pm Operator: 209 GALOS Sample : gems scan 12/14 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Isooctane, (ethenyloxy)- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

35.57 0.91 ug/1 116317 Perylene-d12 37.12

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Isooctane, (ethenyloxy) - 156 C10H20O 037769-62-3 22 2 1-Decene, 4-methyl- 154 C11H22 013151-29-6 22 3 Octane, 1,1’ - oxybi s - 242 C16H340 000629-82-3 14 4 2-Cyclohexen-1-ol Abundance 7 _____________ Scan 3326 (35.574 mln): 30489.D (-) 98 C6H10O 000822-67-3 14 m/z 185.10 100.00% 185 57 70 5000 43 112 83 98 • i ' ' ‘ ■ i ‘ ' ■ ‘ l *

1’444I 125 143 166 209 35.20 35.40 35.60 35.80 36.00 281 1 1 1 MW , i 1 i ' ‘ ' I ‘ ‘ ' I ‘ ‘ ‘ ‘ | ‘ ‘ ‘ ' l ‘ | ‘ ‘ j < t i TJ 1’441444’144 m/z 57.00 71.13% miz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #67294: Isooctane, (ethenyloxy)- 57

71 MAA444AAMA//, , MMM 5000 35.20 35.40 35.60 35.80 36.00 84 27 42 110 m/z 70.10 58.61% 97 |................................................................................ i ■ ■ ■ • i miz-> 20 40 60 80 100 120 140 iso' 180 266' 220 240 260 280 Abundance #11046: 1-Decene, 4-methyl- 57 71 ———————— 35.20 35.40 35.60 35.80 36.00 5000 112 m/z 71.00 !52.88% 84 97 126 154 i ■ • * ■ i • ■ • • i ■ • • • i ■ ■ i ■ ■ ■ ■ i ■ ■ • • i ■ ■ ■ • i ■ ■ ■ ■ i' ■ ■ ■ i ■'1' 111'11111' I'11111 1 m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #71250: Octane, 1,1-oxybis- ■ i ■ ■ ' ■ r1 1 1 1 I ' 1 1 f I ■ A 43 57 71 35.20 35.40 35.60 35.80 36.00 m/z 55.00 51.59% 5000 27 84 112 — 4 ‘9711»111 * 1 1 1 143 224 ■ ■ i ' 1 ■ • i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ■ '1 11 1 1 ' 11 1 11 I 1 1 1111 1 m/z~> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 35.20 35.40 35.60 35.80 36.00

30489.D GCMS1126.M Wed Jan 16 08:27:27 2002 Page 3

NYC-WTC_000017967