GCMS analysis log for sample AD30695, Jan 2002

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Library Search Compound Report

Data File C: \HPCHEM\ 1 \DATA\DEC3 101\30695.D Vial: 32 Acq On 1 Jan 2002 6:59 pm Operator: 209 GALOS Sample gems scan 12/19 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 8 1-Decene, 2,4-dimethyl- Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

35.57 0.68 ug/1 77417 Perylene-d12 37.12

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Decene, 2,4- dimethyl- 168 C12H24 055170-80-4 16 2 3-Piperidinone, 1-acetyl-6-methyl- 155 C8H13NO2 054751-97-2 14 3 Propanedioic acid, hexyl-, diethyl 244 C13H2404 005398-10-7 14 4 Nonane/ 4-methyl- 142 C10H22 017301-94-9 12 Abundance / Scan 3326 (35.574 min): 30695.D (-) m/z 185.10 100.00% 185 57 70 43 5000 112 147 83 98 221 281 35.20 35.40 35.60 35.80 36.00 mlz~> 40 — 60 hluhl 80 —— , 133 I i ■ । ‘ । • 100 120 140 160 180 200 220 240 208 | •1+14’18 2.4 m/z 260 57.0,0 280 75.30% Abundance #14795:1-Decene, 2,4-dimethyl- 43 5 7

83 5000 114 i "11it । IITTrT—rr 11 ■ 70 ! 35.20 35.40 35.60 35.80 36.00 112 m/z 70.00 67.16% 97 _________' i 168 _______________________ i ' ■ ■ ■ i 1 ■' I ■ ■ ' i ■ ■ ■ 1 i ‘ ■ ‘ ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i ‘ ■ i ■ ■ ■ ■ i ' ' 1 • i ' ' mlz—> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #11169 3-Piperidinone, 1-acetyl-6-methyl- 70 112 . .So. 35.20 35.40 35.60 35.80 36.00 5000 m/ z 55.00 66.59% 155

L 56 98 84 127 ■ • i ■ ■ * ■ i1 •' ■ ।1' * ■ i ■ ■ I ‘ ■ i ■ 1 ■ ‘ i • 1 ■ 1 i ' ‘ 1 • i ' ‘ ■ i ■ ' ' ■ i ■ • ■ ■ i ■ • ■ ■ i • ■ miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #32687: Propanedioic acid, hexyl-, diethyl ester AAm MA A n/ “WW 57 70 35.20 35.40 35.60 35.80 36.00 m/ Z 71.10 60.73% 5000 83 112

42

miz-> - I •‘‘'I 40 60 80 98 fl

100 | 199 217 1 i 1 1 ■ • i ■ ■ ‘ • i 1 ' ' ' i ■ ■ ■ ■ i ■ ‘ ■ ■ i • ■ • ■ i ■ ‘ 1 ‘ I ■ ' ■ 1 i 1 ' 120 140 160 180 200 220 240 260 280 .................. / 344 35.20 35.40 35.60 35.80 36.00

30695.D GCMS1126.M Wed Jan 23 08:34:00 2002 Page 8

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