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GCMS analysis log for sample AD30695, Jan 2002

Machine-extracted title · confidence 100%

Automated laboratory log recording GCMS analysis of sample AD30695 including detection of unknown compounds and surrogates.

NYC-WTC_000018107–000018122

Folder label: “GCMS X 12/27/01 A 1/16/02

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Scanned page image, NYC-WTC_000018122
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NYC 9/11 Public Portal Document

Tentatively Identified Compound (LSC) summary

Operator ID: 209 GALOS Date Acquired: 1 Jan 2002 6:59 pm Data File: C:\HPCHEM\1\DATA\DEC3101\30695.D Name: gems scan 12/19 Mise: Method: C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title: 209 625/TCLP calibration table Library Searched: C:\DATABASE\NBS75K.L

TIC Top Hit name RT EstConc Units Area IntStd ISRT ISArea ISConc

Pentane, 3 -methoxy- 7.62 3.5 ug/1 817376 ISTD01 11.68 4675410 20.0 Cyclotetrasiloxane, 11.13 1.2 ug/1 273954 ISTD01 11.68 4675410 20.0 Cyclopentasiloxane, . 14.30 1.6 ug/1 456884 ISTD02 15.28 5891860 20.0 Cyclohexasiloxane, d 17.45 1.9 ug/1 555243 ISTD02 15.28 5891860 20.0 3-Isopropoxy-1, 1,1,7 20.28 1.0 ug/1 337096 ISTD03 20.56 6456610 20.0 Benzoic acid, 2,5-bi 22.80 0.6 ug/1 186974 ISTD04 24.99 5946540 20.0 Trisiloxane, 1,1,1,5 26.89 0.2 ug/1 68079 ISTD04 24.99 5946540 20.0 1-Decene, 2,4-dimeth 35.57 0.7 ug/1 77417 ISTD06 37.12 2274000 20.0

30695.D GCMS1126.M Wed Jan 23 08:34:00 2002

5

NYC-WTC_000018122

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NYC-WTC_000018122Source: NYC Law Department, mirrored locally

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