Automated laboratory log recording GCMS analysis of sample AD30695 including detection of unknown compounds and surrogates.
NYC-WTC_000018107–000018122Folder label: “GCMS X 12/27/01 A 1/16/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Library Search Compound Report Data File C:\HPCHEM\1\DATA\DEC3101\30695.D Vial: 32 Acq On 1 Jan 2002 6:59 pm Operator: 209 GALOS Sample gems scan 12/19 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 7 Trisiloxane, 1,1,1,5,5,5-hexam Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T.
26.89 0.23 ug/1 68079 Phenanthrene- dl 0 24.99
Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Trisiloxane, 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 47 2 3-Isopropoxy-1, 1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 45 3 Mercaptoacetic acid, bis(trimethyls 236 C8H20O2SSi2 006398-62-5 25 4 3-Is ropoxy-1,1, 1,5,5,5-hexamethy1 354 C12H3404Si4 072182-11-7 23 Abundance / Scan 2380 (26.889 min): 30695.D (-) m/z 73.00 100.00% 73
5000 147 221 281 — 45 1 100 —IT 117 1 ,, 1911 .... .. , 327355...... 429 ....... 150 200 ' 250 ' 300 ' ‘ 350 ' 400 450 ' 500 550 ' 26.60 26.80 27.00 27.20 m/z 147.10 32.25% m/z~> 50 Abundance #52459: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trimet 73 147 281 5000 26.60 26.80 27.00 27*20 20- | 369 m/z 281.10 18.60% ! miz-> ilii 50 100 150 443_ 450 200 250 300 350 400 500 550 Abundance #60503: 3-Isopropoxy-1,1.1.7.7,7-hexamethyJ-3.5,5-tris(trim 73
5000 147 m/z "7 26.60 26.80 27.00 27.20 14.73%
221 281 327 415 i ■ 519 561 4-I****I*++I***I*’’*I’-41++*1*’’’I4*--II’III1III4 mz-> 50 11 100 1 150 200 250 300 * * 350 400 450 500 550 Abundance #30949: Mercaptoacetic acid, bis(trimethylsilyl)- • ‘ 1 I ‘ * I ’ ‘ ‘ I * ‘ ‘ I ' ' 1 * 73 26,60 26.80 27.00 27.20 147 m/z 74.00 10.05% 5000 221
miz—> ++ 45
50 104 1 ■ i'1 ■ 100 ' 150 , 193 I __________________________________________________ ‘ ‘ ‘ ■ i • f ■ • i • ' • ' i • ■ ‘ ■ i ' ' ' • I 1 1 1 ' I 1 1 1 1 I ' 1 1 ' I ' 1 200 250 300 350 400 450 500 550 26.60 26.80 27.00 27.20
30695.D GCMS1126.M Wed Jan 23 08:33:55 2002 Page 7
NYC-WTC_000018120
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NYC-WTC_000018716
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30933 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018093
Automated laboratory log recording GCMS analysis of sample AD30694 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018155
Automated laboratory log recording GCMS analysis of sample AD30713 including detection of unknown compounds and surrogates.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018605
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30705 conducted on January 28, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018174
Automated laboratory log recording GCMS analysis of sample AD30714 including detection of unknown compounds and surrogates.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018664
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30907 conducted on January 28, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018624
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30904 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018733
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30934 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018194
Automated laboratory log recording GCMS analysis of sample AD30605 including detection of unknown compounds and surrogates.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018754
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30935 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036842
GCMS analysis report for sample AD29670 listing unknown compounds and surrogate recovery data from January 28, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036542
Laboratory commentary noting detection of bis(2-Ethylhexyl)phthalate in sample AD29520 and blank on January 25, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000018058
Document with unreadable text from the GCMS X folder series in DEP Box 16.
Filed in the same folder
NYC-WTC_000018059
Calibration verification report using DFTPP standard for GCMS instrument performance check on January 1, 2002.
Filed in the same folder
NYC-WTC_000018060
Laboratory report documenting GCMS calibration analysis of sample AD30694 conducted on January 18, 2002.
Filed in the same folder
NYC-WTC_000018064
Reference data table listing response factors and concentrations for organic compounds used in GCMS analysis of sample AD30694.
Filed in the same folder
NYC-WTC_000018069
Blank analysis report showing non-detectable levels of target organic compounds in sample AD30694.
Filed in the same folder