NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\HPCHEM\1\DATA\DEC3101\30705.D vial: 46
Acq On 2 Jan 2002 9:30 am Operator: 209 GALOS
Sample gems scan 12/19a Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Library : C:\DATABASE\NBS75K.L
*********************************************************************
Peak Number 8 Trisiloxane, 1,1,1,5,5,5-hexam Concentration Rank 8
R.T. EstConc Area Relative to ISTD R.T.
26.89 0.47 ug/1 142875 Phenanthrene-dl0 24.99
Hit# Of 5 Tentative ID MW MolForm CAS# Qual
1 Trisiloxane, 1, 1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 42
2 Ethanedioic acid, bis(trimethylsily 234 C8H18O4Si2 018294-04-7 38
3 3-Isopropoxy-1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 34
4 2-Pentenoi acid, 2-[(trimethylsily 260 CllH24O3Si2 055045-17-5 23
Abundance Scan 2380 (26.890 mln): 30705.D (-) m/z 73.0P 100.00%
73
5000
147
221 281
45 117’ 191 249 327 355 401 429 26.60 26.80 27.00 27.20
TI m/z 147.op 30.81%
miz-> 50 100 150 200 250 300 350 400 450 500 550
Abundance #52459: Trisiloxane, 1,1,1,5.5,5-hexamethyl-3,3-bis[(trimet
73 147
5000
281
369
A
26.60 26.80 27.00 27.20
m/z 281.op
1 1 I 1 1
17.51%
207
miz-
1
‘*1*1**-I‘**1*
50 100 150 200
1
24944338-
250 300 350 400 450 500 550
Abundance #30580: Ethanedioic acid, bis(trimethyisilyi) ester
73 147
* * * i * * * • i • * • * n * • • i • • * *'
26.60 26.80 27.00 27.20
5000 m/z 221.0,5 15.30%
45
miz-> 50 ‘ 100>
.190219
150 200 250 300 350 ‘ 400 450 500 ' 550
Abundance #60503:3-lsopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim / \
73 26.60 26.80 27.00 27.20
m/z 74.00 9.47%
5000
147
221 281 20- 24E
. .... ., , [.. J' u.. . ... 519 561 .............
■ • i ‘
1 \................
‘ ‘ i ' ■ • ■ i 1 1 1 1 1 1 1
m/z—> 50 100 150 200 250 300 350 400 450 500 550 26.60 26.80 27.00 27.20
30705.D GCMS1126.M Fri Jan 25 11:27:29 2002 Page 8
NYC-WTC_000018619
OCR can misread numbers and units. Confirm readings against the page image before using them.