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GC/MS analysis results for sample AD30705, Jan 28 2002

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Laboratory report documenting gas chromatography mass spectrometry results for sample AD30705 conducted on January 28, 2002.

NYC-WTC_000018605–000018623

Folder label: “GCMS X 12/19/01 A 1/2/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\DEC3101\30705.D vial: 46 Acq On 2 Jan 2002 9:30 am Operator: 209 GALOS Sample gems scan 12/19a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 8 Trisiloxane, 1,1,1,5,5,5-hexam Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T.

26.89 0.47 ug/1 142875 Phenanthrene-dl0 24.99

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Trisiloxane, 1, 1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 42 2 Ethanedioic acid, bis(trimethylsily 234 C8H18O4Si2 018294-04-7 38 3 3-Isopropoxy-1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 34 4 2-Pentenoi acid, 2-[(trimethylsily 260 CllH24O3Si2 055045-17-5 23 Abundance Scan 2380 (26.890 mln): 30705.D (-) m/z 73.0P 100.00% 73

5000 147 221 281 45 117’ 191 249 327 355 401 429 26.60 26.80 27.00 27.20 TI m/z 147.op 30.81% miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #52459: Trisiloxane, 1,1,1,5.5,5-hexamethyl-3,3-bis[(trimet 73 147

5000 281

369 A 26.60 26.80 27.00 27.20 m/z 281.op 1 1 I 1 1

17.51% 207 miz- 1 ‘*1*1**-I‘**1* 50 100 150 200 1 24944338- 250 300 350 400 450 500 550 Abundance #30580: Ethanedioic acid, bis(trimethyisilyi) ester 73 147 * * * i * * * • i • * • * n * • • i • • * *' 26.60 26.80 27.00 27.20 5000 m/z 221.0,5 15.30% 45

miz-> 50 ‘ 100> .190219 150 200 250 300 350 ‘ 400 450 500 ' 550 Abundance #60503:3-lsopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim / \ 73 26.60 26.80 27.00 27.20 m/z 74.00 9.47% 5000 147 221 281 20- 24E . .... ., , [.. J' u.. . ... 519 561 ............. ■ • i ‘ 1 \................ ‘ ‘ i ' ■ • ■ i 1 1 1 1 1 1 1 m/z—> 50 100 150 200 250 300 350 400 450 500 550 26.60 26.80 27.00 27.20

30705.D GCMS1126.M Fri Jan 25 11:27:29 2002 Page 8

NYC-WTC_000018619

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