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GC/MS analysis results for sample AD30705, Jan 28 2002

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Laboratory report documenting gas chromatography mass spectrometry results for sample AD30705 conducted on January 28, 2002.

NYC-WTC_000018605–000018623

Folder label: “GCMS X 12/19/01 A 1/2/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\DEC3101\30705.D Vial: 46 Acq On 2 Jan 2002 9:30 am Operator: 209 GALOS Sample gems scan 12/19a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 7 Decafluorotriphenylphosphine Concentration Rank 10

R.T. EstConc Area Relative to ISTD R.T.

26.22 0.44 ug/1 134956 Phenanthrene-dl0 24.99 Hit# of ---- -------- —-- -==--e- 04 MW Mol Form Tentative ID 5 leIILaLIve LD . CAS# Qual 1 Decafl uoro t r iphenylphosphi ne 0 442 C18H5F10P 005074-71-5 99 2 Hydrazine,—(pentafluerophenyl)— 198 C6H3F5N2 000828-73-9 14 3 Hydrazinecarbodithioic acid, 2-phen 198 C8H10N2S2 050878-38-1 9 4 Benzeneacetonitrile, .alpha.-hydrox 225 C14H11NO2 052315-06-7 9 Abundance Scan 2307 (26.220 min): 30705.D (-) m/z 197.95 100.00% 198 69 127 442 5000 255

5) IC 7 | 224 275 .uuqll,l 148766,1 atk J j „ 1 296 323 •*1*‘I**I‘ T 25.80 26.00 26.20 26.40 26.60 m/z 69.00 63.66% mlz-> 50 100 150 200 250 300 350 400 Abundance #56592: Decafluorotriphenylphosphine 198

51 77 5000 127 442 25.80 26.00 26.20 2640 26.60 255 1C7 275 m/ z 77.0,5 53.15% ] 224 1 J I iI 296323 365 423 T m/z-> 50 100 150 200 250 300 350 400 ' Abundance #22159: Hydrazine, (pentaflucropheny!) 198 ----- 25.80 26.00 26.20 26.40 26.60 5000 155 m/z 127.00 52.51%

m/z-> 30 50 69 93100 117 1 150 ' '260' ' 250 ‘300 350 400 Abundance #22221: Hydrazinecarbodithioic acid, 2-phenyl-, methyl ester 198 25.80 26.00 26.20 26.40 26.60 m/z 442.0,0 46.76% 5000

.. e 91 150 4295,4424, 1 • i miz-> 50 100 150 200 250 300 350 400 25.80 26.00 26.20 26.40 26.60

30705.D GCMS1126.M Fri Jan 25 11:27:25 2002 Page 7

NYC-WTC_000018618

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NYC-WTC_000018618Source: NYC Law Department, mirrored locally

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