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GCMS analysis results for sample AD31466, Feb 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD31466 conducted on February 11, 2002.

NYC-WTC_000018405–000018415

Folder label: “GCMS X 12/27/01 A 1/16/02

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Scanned page image, NYC-WTC_000018413
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\JAN1602\31466.D Vial: 25 Acq On : 17 Jan 2002 12:04 pm Operator: 209 GALOS Sample : gc/ms scan 12/28 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Decafluorotriphenylphosphine Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

26.02 0.50 ug/1 148461 Phenanthrene-dl0 24.78

Hit# of 5 Tentative ID C MW MolForm CAS# Qual

1 Decafluorotriphenylphosphine 442 C18H5F10P 005074-71-5 99 2 Dibenzofuran, 2-methoxy- 198 C13H10O2 020357-70-4 25 3 Dibenzothiophene, 3-methyl- 198 C13H10S 016587-52-3 14 4 .beta.-Carbol! e, 7-hydroxy-1-methy 198 C12H1ON20 000000-00-0 14 Abundance Scan 2285 (26.025 min): 31466.D (-) m/z 197.95 100.00% 198 69 127 442 5000 255 275 5) 107 224 [ 296 323 365 423

m&~> 1 adqlt 50 117.1.4 100 150 2001 llL4 250 300 350 400 25.60 25.80 26.00 26.20 26.40 m/z 69.00 69.79% Abundance #74461: Decafluorotriphenylphosphine 198

127 442 11.01 N m 5000 77 51 255 25.60 25.80 26.00 26.20 26.40 275 m/z 77.05 61.62% 107 224 I 296 323 365 423 ‘ I ' 1L—1Ir-T—1—. । . 1)—IT m/z-> 50 100 150 200 250 300 350 400 Abundance #22452 Epenzcfuran 2-ethox, 198 . ............ .................................... 155 25.60 25.80 26.00 26.20 26.40 $ 127 m/z 442.00 5000 54.59% 101 “i

m/z-> 50 100 150 200 250 300 350 400 Abundance #22461: Dibenzothiophene, 3-methyl- rT' ■ 1 1 I • ’ ‘ * I * ’ 198 25.60 25.80 26.00 26,20 26.40 m/z 127.00 49.39% 5000

L 99 139165 J 1 1—[—1—T—I—1—|—I T ......... ....................................... m/z~> 50 100 150 200 250 '300‘ 350 400 25.60 25.80 26.00 26.20 26.40

31466.D GCMS0103.M Thu Feb 07 12:42:33 2002 Page 2

NYC-WTC_000018413

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NYC-WTC_000018413Source: NYC Law Department, mirrored locally

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