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← Document results/DEP Box 16/GCMS X 12/31/01 A 1/18/02
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GCMS blank analysis, sample AD31432, Jan 2002

Machine-extracted title · confidence 95%

Blank analysis report for DEP sample AD31432 showing non-detect levels for volatile organic compounds from January 22, 2002.

NYC-WTC_000016555–000016563

Folder label: “GCMS X 12/31/01 A 1/18/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\JAN1802\LB.D Vial: 4 Acq On : 18 Jan 2002 6:34 pm Operator: 209 GALOS Sample : gc/ms scan 12/31 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Phenanthrene-diO Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

24.91 0.25 ug/1 77852 Phenanthrene-dl0 24.77

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene-d 001517-22-2 59 188 C14D10 2 Selenide, ethy1 1-methyl-1-penten-3 188 C8H12Se 025128-48-7 33 3 Cyclohexanone, phenylhydrazone 188 C12H16N2 000946-82-7 28 4 Pentacycl 8.4.0.0(3,7) .0(4,14) .0(6 188 C14H20 __ 000000-00-0 28 Abundance Scan 2164 (24.915 min): LB.D (-) m/z 188.10 100.00% 188

5000

80 94132 160 | | 24.60 24.80 25.00 25.20 ' 253 268 miz-> 36 TTIt 40 52.6096.111, . .............rr.... h"a 80 100 120__ 140 160 180 200 220 240 260 m/z 94.00 21.97% Abundance #19958: Phenanthrene-d10 188

5000 24.60 24.80 25.00 25.20 ‘ ' 160 m/z 184.10 19.82% 80 94 00 ’! 11BBT9mm2er - miz-> 40__ 60 80 100 120 140 160 180 200 220 240 260 Abundance 41573S. Menide chyl 1-mettrtl-penton- 188 ■ ' I ' 1 r ‘ 1 1 ' 1 ' I ' 1 ‘ 1 I ' ■ ‘ ‘ I 24.60 24.80 25.00 25.20 5000 m/z 189.10 18.35% 79 169 145 173 I | ll ill 1111111111' > ।11■'।■■■■।■i1'■•।1'■■।1,111। ।11 ■ m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #19927: Cyclohexanone, phenylhydrazone 188 24.60 24.80 25.00 25.20 93 m/ z .95 16.27% 5000 65 77 106 146 |i | J20 132 15917Q ■ ■ i ■1 ■ 11 ■ ■ ■ ■ i ■1 ’ * I ‘ 1 ' * I * ‘ ' I ‘ ‘ ‘ * 1 ‘ 1 m/z-> 40 60 80 100 120 140 160′ 180 200 220 240 260 24.60 24.80 25.00 25.20 '

LB.D GCMS0103.M Wed Feb 06 15:44:02 2002 Page 2

NYC-WTC_000016562

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NYC-WTC_000016562Source: NYC Law Department, mirrored locally

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GCMS blank analysis report, Feb 2002 · Box DEP Box 12

NYC-WTC_000005159

Blank sample analysis report confirming no contamination above method detection limits for target compounds analyzed on February 1, 2002.

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