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Document / 344 pages

DEP GCMS data table, Jan-Feb 2002

Machine-extracted title · confidence 90%

Large multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

NYC-WTC_000004149–000004492

Folder label: “GCMS X 12/18/01, 2/8/02 A 2/10/02, 1/10/02, 1/14/02

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Scanned page image, NYC-WTC_000004262
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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\JAN2 502\30649.D Vial: 34 Acq On : 25 Jan 2002 9:55 pm Operator: 209 GALOS Sample : REINJECT Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 9 Phenanthrene-diO Concentration Rank 18

R.T. EstConc Area Relative to ISTD R.T.

24.90 0.23 ug/1 210903 Phenanthrene-dl0 24.77

Hit# of 5 TentativeIB MW MolForm CAS# Qual

1 Phenanthrene-diO 188 C14D10 001517-22-2 80 2 Pentacyclef[8.4.0.0 (3,7) .0(4,14) .0(6 188 C14H20 000000-00-0 36 3 Selenide, ethyl 1-methyl-1-penten-3 188 C8H12Se 025128-48-7 33 _4 4-Methyl-2-(3-fluorophenyl)pyrimidi 188 C11H9FN2 076128-66-0 33 Abundance C Scan 2163 (24.904 min): 30649.D (-) m/z 188.10 100.00% 188

5000

80 94 24.60 24.80 25.00 25.20 42 52 66 132 146 160 170 , 11 |,11 108 118207 221 TTHTH 1 ■r " • i'1 ‘1 ‘ i 1111»11 fl 111111 hi । ri H |‘i 1111‘■I I । । | I ।। i । । । । i । i m/z 189.10 16.37% miz-> 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 200 210 220 Abundance #19958: Phenanthrene-d10 188

5000 24.60 24.80 25.00 25.20 m/z 80.05 14.24%

m/z-> .... ... ^,...1...".............. T.... il. 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 220 ■ i" " r " ■ i ■ ‘ ■ i

Abundance #19959: Pentacyclo[8.4.0.0(3,7),0(4.14).0(6,11)tctradecane 188

24.60 24.80 25.00 25.20 5000 m/z 184.10 13.70% 7 92 106 117 131 145 159 173 । ।।।...,।।।।।।।।।।।।।।.।। m/z->__ 30 40 50 60 70 80 90 100110120130140 150160170180 190 200 210 220__ Abundance #19733: Selenide, ethyl 1-methyl-1-penten-3-ynyl i 188 24.60 24.80 25.00 25.20 m/z 94.00 13.11% 5000 79 159

m/z—> I" " i" " r ■" i" " i1 ■' i" " r ■" i' ■" i" " i" " i" " I ‘'11" 145 11173 ’ouun—ItI0——E-I"IIIT 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 200 210 220 24.60 24.80 25.00 25.20

30649.D GCMS1126.M Mon Jan 28 12:18:32 2002 Page 9

NYC-WTC_000004262

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NYC-WTC_000004262Source: NYC Law Department, mirrored locally

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