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GCMS unknowns analysis results for sample AE07486, April 2002

Machine-extracted title · confidence 100%

DEP laboratory report showing GCMS unknowns analysis results for sample AE07486 conducted on April 23, 2002.

NYC-WTC_000047101–000047110

Folder label: “GCMS X 4/1/02 A 4/20/02

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Scanned page image, NYC-WTC_000047109
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\APRI802\7486.D Vial: 19 Acq On : 20 Apr 2002 11:07 am Operator: Sample : gc/ms scan 4/1 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0419.M (RTE Integrator) Title : 209 625/TCLP calibration table Library- : C:\DATABASE\NBS75K.L

Peak Number 2 Phenanthrene-diO Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

25.73 0.22 ug/1 36431 Phenanthrene-dl0 25.59

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Phenanthrene -d1 07 188 C14D10 001517-22-2 72 2 Naphthalene/ 2,6-dimethoxy- 188 C12H1202 005486-55-5 40 3 4H-Pyrido [l, 2-a] pyrimidin-4-one, 3- 188 C11H12N2O 057773-19-0 40 4 Anthracene d10- 188 C14D10 001719-06-8 39 Abundance Scan 2253 (25.726 min): 7486.D (-) m/z 188.10 100.00% 188

5000 ----- 42 66 80 94 158 25.40 25.60 25.80 26.00 1 1 | | TI ■ I | I | | | | ' I I ■ pl I | i i I I | I 1 I I | I I I i t | r r' I I | I I | I | I | | I | | r | | | |"| | | | | ri r I TET rn/z 189.10 13.09% m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19958: Phenanthrene-d10 188

5000 ......................................... ............ 25.40 25.60 25.80 26.00 m/ z 93.95 11.35% 80 94 160 66 n/z-> ■ i ■ > ■ ■। ■ ■ ■ • । 40 50 60 > I• । ■ 70 80 H IBB*II*0** 90 100 110 120 130 140 150 160 170 180 190 T’TT

Abundance #19908: Naphthalene, 2,6-dimethoxy- 188 . — 173 145 25.40 25.60 25.80 26.00 5000 m/z 158.05 10.85% 102 130

m/z-> 76 94 114 TIUUTIIUTTTTTT —PTP TITH । ■ ir ■ ■ ■ i ■ ■ ■ > । ■ 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 .157.... u Abundance #19873: 4H-Pyrido(1,2-a]pyrimidin-4-one, 3-ethyl-6-methyl- 145 188 25.40 25.60 25.80 26.00 173 m/z 92.10 10.30%

5000 92

65 159 .. Pp TTT " i" ■ ■ i'" ■ ।'1111 ■111 r1111 | 119 132 m/z—> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 25.40 25.60 25.80 26.00

7486.D GCMS0419.M Mon Apr 22 12:35:41 2002 Page 2 NYC-WTC_000047109

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NYC-WTC_000047109Source: NYC Law Department, mirrored locally

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