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GCMS results sample AE05749, April 2002

Machine-extracted title · confidence 100%

GCMS analysis report for sample AE05749 showing surrogate recovery and unknown compounds from April 2002.

NYC-WTC_000047979–000048003

Folder label: “GCMS X 4/8/02 A 4/18/02

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Scanned page image, NYC-WTC_000047987
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C : \HPCHEM\ 1\DATA\APRO 102\5749.D Vial: 28 Acq On 3 Apr 2002 3:58 am Operator: Sample gc/ms scan 3/12 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 2 Phenanthrene-diO Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

25.77 0.22 ug/1 40434 Phenanthrene-dl0 25.64

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene-d10 188 C14D10 001517-22-2 72 2 Antipyrine 188 C11H12N2O 000060-80-0 42 3 Anthracene-dlO- 188 C14D10 001719-06-8 40 4 Naphthalene, 1,7-dimethoxy- 188 C12H1202 005309-18-2 38 Abundarce (.... “ " .. . ' ..... Scan 2258 (25.773 min): 5749.D (-) I m/z 188.10 100.00% 188

5000

66 80 94 158 . 25.40 25.60 25.80 26.00 26.20 1 | 1 | ' 1 I ' | 1 I | । 1 I I I I 1 | 1 1 1 I | I ' I I | IITH " ........... 'll Trt 1 1 ' 1 ' I L m/z 189.05 13.74% m/z-2 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19958: Phenanthrene-d10 188

5000 TIT I-’"1" r 1 1 1 1 1 1 1 1 25.40 25.60 25.80 26.00 26.20 80 94 160 I m/ z 18 . 05 12.17% 66 PPTP ------- m/z-> 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance r _ A ■' yt G 188 96 25.40 25.60 25.80 26.00 26.20 5000- 77 m/z . 00 9.61% 56 105 84 159 173 1 1 ' 1 ' 1 I ' ' 1 ' 1 1 1 1 ' 1 1 ' ' 1 r 1 ' ' I ' 1 1 ‘ I 1 1 1 1 1 1 IITTFFPIT i i i i I i । i । I i | i . I I-I ri I i i i i I i i m/z-> 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19957: Anthracene-d10- 1 i ' TIIdIIII 188 25.40 25.60 25.80 26.00 26.20 m/ Z . 95 8.45% 5000

66 80 94 160 -PPPH - -rp-r-r-r-p- TIm rl 1 1 1 1 I"T‘"I ■' I ‘ m/z-> 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 25.40 25.60 25.80 26.00 26.20

5749.D GCMS0403.M Fri Apr 05 10:41:13 2002 Page 2

NYC-WTC_000047987

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NYC-WTC_000047987Source: NYC Law Department, mirrored locally

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