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GCMS analysis results for sample AE08015, April 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE08015 conducted on April 24, 2002, including surrogate recovery data.

NYC-WTC_000047691–000047700

Folder label: “GCMS X 4/4/02 A 4/12/02

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Scanned page image, NYC-WTC_000047699
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\APRI102\8015.D Vial: 21 Acq On : 12 Apr 2002 10:03 am Operator: Sample : gc/ms scan 4/4 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 2 Phenanthrene-diO Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

25.75 0.23 ug/1 38997 Phenanthrene-dl0 25.60 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene-diO 188 C14D10 001517-22-2 3 2 Anthracene-d10- 188 C14D10 001719-06-8 56 3 Cyclohexanone, phenylhydrazone 188 C12H16N2 000946-82-7 9 4 Antipyrine 188 C11H12N2O 000060-80-0 9 Abundance Scan 2255 (25.750 min): 8015.D (-) m/z 188.10 100.00% 188

5000

80 94 ' ‘ I 1 1 r 1 i ' 1 ' 1 i 1 ‘ ' i ' 1 1 1 i ' 25.40 25.60 25.80 26.00

m/z-> 40 44 50 60 66 70 L I'' ‘/‘11' I 80 90 100 110 120 130 140 150 160 170 180 190 160 , - I’r L m/ Z 189.10 16.03%| Abundance #19958: Phenanthrene-d10 188

5000 I-' 25.40 25.60 25.80 26.00 m/ Z 94.00 15.85%I

n/z-> A 80 94

40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 160 l Abundance #19957: Anthracene-d10- 188 ----- 25.40 25.60 25.80 26.00 5000 m/z 79.95 11.96%

80 94 160 66 1111 •11■■>।■ j ■ 1 ■ | 1 ■ 1 ' | • 1 1 1 | 1 1 1 1 | । । 1 1 | 1 1 I ITI I I | i ni | > I m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19927: Cyclohexanone, phenylhydrazone -- 188 25.40 25.60 25.80 26.00 93 m/Z 184.00 9.88% 5000 65 77 106 145 ..... I,,, I ,, 120 132 ---PP I ' ' | ■ * I 1 1 159 170 11’1 '''' I''r 11 0 m/z—> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 25.40 25.60 25.80 26.00

8015.D GCMS0412.M Tue Apr 16 12:07:37 2002 Page 2

NYC-WTC_000047699

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NYC-WTC_000047699Source: NYC Law Department, mirrored locally

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