GCMS surrogate recovery data for sample AE07765, April 2002

Machine-extracted title · confidence 100%

Record of surrogate compound recovery rates for sample AE07638 analyzed on April 18, 2002.

NYC-WTC_000040269–000040278

Folder label: “GCMS X 4/3/02 A 4/10/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\APRI102\7765.D Vial: 14 Acq On : 12 Apr 2002 3:10 am Operator: Sample : gc/ms scan 4/3 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 2 Phenanthrene-diO Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

25.75 0.21 ug/1 30680 Phenanthrene-dl0 25.60

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene-d10 X/ 001517-22-2.91) 188 C14D10 2 Anthracene-dl0- 001719-06-890 188 C14D10 3 Cyclohexanone , phenyl hydra zone 188 C12H16N2 000946-82-7 53 4 4-Fluoro-/6-methyl-2-phenylpyrimidin 188 C11H9FN2 000000-00-0 45 Abundance Scan 2255 (25.750 min): 7765. D (-) m/z 188.10 100.00% 188

5000

1 ' 1 1 1 i 1 ’ i 1 1 1 1 i ' 1 1 1 i 1 80 94 160 25.40 25.60 25.80 26.00

miz-> 40 44 50 60 66 70 80 ‘ 1 । ■ j • ■ ■ ■ । । । • ■ ■ ■ । ■ ■ ■ • ।

90 100 110 120 130 140 150 160 170 180 190 ■ 11 .... 4 I I m/z 187.10 22.38%

Abundance #19958: Phenanthrene-d10 188

........................................................

5000 25.40 25.60 25.80 26.00 m/z 189.10 14.43% 66.. 80L — 94 TPPITTTTWTTTTT 160 ■' r ' miz-> 40 50 60 70 80 90 100 11 120 130 140 150 160 170 180 190 Abundance #19957: Anthracene-d10- 188 1 T । 1 ■ ■ r । > i • 1 | 1 1 1 i । ■ . > 1 । i 25.40 25.60 25.80 26.00 5000 m/z 184.10 12.82% fl 80 94 160 66 t i i | i ■ i i । I L i I — । । i n i । । > । । । i n i | i i H | n — 1111111 > ।1 - 1 11' 1 mfe-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19927: Cyclohexanone, phenylhydrazone ..... J................. ' ' I 1 1 ' ' I Tdn I I | I ! I ! | I 188 25.40 25.60 25.80 26.00 93 m/ z 94.00 12.19%

5000 65 77 106 145 120 132 | 159 170 1........... _ T I I TT I T t TTT r ’ 1111' I'b'111 11’0’10111, TIET r 1111' * ’/'i - * - • । ■ T’t । ■ 1 ■ ■ । ■ 1 । । j । । > 1 ( । 1 1 i 1 1 m/z—> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 25.40 25.60 25.80 26.00

7765.D GCMS0412.M Fri Apr 12 09:28:02 2002 Page 2

NYC-WTC_000040277

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