TCLP calibration table review document, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\APR1202\8481.D Vial: 26 Acq On : 16 Apr 2002 9:08 am Operator: Sample : gc/ms scan 4/10 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 9 Phenanthrene-diO Concentration Rank 9 R.T. EstConc Area Relative to ISTD R.T. 25.75 0.23 g/1 47239 Phenanthrene-dl0 25.61

Hit# of 5 Tentative7 ID MW MolForm CAS# Qual 1 Phenanthrene-d102/77 188 C14D10 001517-22-2 74 2 Anthracene-diO- X 188 C14D10 001719-06-8 72 3 Naphthalene, 2,6-dimethoxy- 188 C12H1202 005486-55-5 50 4 2-Quinolinecarboxaldehyde, 8-hydrox 188 C10H8N2O2 005603-22-5 40 Abundance ‘ Scan 2256 (25,754 min): 8481 .D (-) m/z 188.10 100.00% 188

5000 | | I I I 4 s — | I I ! i—।—!—i—i—i—[—r

42 52 66 8|° 9|4 146 160 1 25.40 25.60 25.80 26.00 ■ 1111 ■ 111 ■ ■ 1111 > । ■ > 1111 > 11111 ■ 111 >>> 11 > 1111111111111111111111111111111111 H IT m/ z 18 9.10 15.53% m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19958: Phenanthrene-d10 188

5000 ■ i ’ 1

25.40 25.60 25.80 26.00 m/ Z 80.05 14.00% 66 80 94 160 m/z-> p — 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19957: Anthracene-d10- 188 i | i f i I । । I - | i i i i । i । । । [ r

25.40 25.60 25.80 26.00 5000 m/ z 94.00 13.19%

80 94 160 66 I mm i T i n i । । । n | n i r n i T PT1 TIM I " 11 " 11. Ir m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19908: Naphthalene, 2,6-dimethoxy- I-1 I I ll ).......... [ I I I I [ I I I I [ I I I I I 1 188 25.40 25.60 25.80 26.00 173 m/ Z 184.10 9.15% 145 5000 102 114 130 76 94 1 "] i n i । । । । । । । । » । । r । I । । n rd । i I । । । .... ........ r iI1iri|। । ।r 157 11111111'1111111111 TTTT t [ । । । * । । I 1 i । । । । । l r m/z—> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 25.40 25.60 25.80 26.00

8481.D GCMS0412.M Fri Apr 26 12:47:28 2002 Page 9

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