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GCMS calibration table and instrument parameters, Apr 2002

Machine-extracted title · confidence 90%

Instrument calibration records and method parameters for GCMS analysis of polycyclic aromatic hydrocarbons.

NYC-WTC_000048583–000048597

Folder label: “GCMS X 4/10/02 A 4/15/02

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Scanned page image, NYC-WTC_000048596
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\APR12O2\8481. D Vial: 26 Acq On : 16 Apr 2002 9:08 am Operator: Sample : gc/ms scan 4/10 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 9 Phenanthrene-diO Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T. 25.75 0.23 ug/1 47239 Phenanthrene-dl0 25.61 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene-d10 188 C14D10 001517-22-2 74 2 Anthracene-diO- 188 C14D10 001719-06-8 72 3 Naphthalene, 2,6-dimethoxy- 188 C12H1202 005486-55-5 50 4 2-Quinolinecarboxaldehyde, 8-hydrox 188 C10H8N2O2 005603-22-5 40 Abundance Scan 2256 (25.754 min): 8481 .D (-) m/z 188.10 100.00%! 188

5000

/ 66 80 94 25.40 25.60 25.80 26.00 42 52 160 TIP 1111111111111111 I I I I I I > I I I I I I I I I I I I I I I 146 I..I I I I I I I I I I I I II I > I I I I I f'l TIT L m/z 189.10 15.53%| m/z-> Abundance 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 A #19958: Phenantbrene-d10 188

5000 , 19s 25.40 25.60 25.80 26.00 TT

m/ z 80.05 14.00 80 94 160 66 A - ...W. rn/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19957: Anthracene-d10- 188

25.40 25.60 25.80 26.00 5000 m/z 94.00 13.19%

66 TPPTPPTTTT 60 T 160 I 11 1 । 1 1 ! I | I । > I | ! ! > I | I I I ! | I ! I ! | ! ! I I | I I I I | I I I l'[ I I I I | I 1 I I | I’l'l'l | "I I I I

n/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19908: Naphthalene, 2,6-dimethoxy- ........ / 1 i ■ 1 ■ ' 1 11 I "1"1 । । । । । । > । । 188 25.40 25.60 25.80 26.00 173 m/Z 184.10 9.15%| 145 5000 102 114 130 76 94 । TI ’I | ''I 1 ■ | ' > > । 157 TIITTTTWWWTTTTPTTT 1 ■ i11'r 1111111'111' — TTT ■ i ■ ■ 1 r i 1 1 1 1 i ‘ ■ ■ i 1 ■ ■ 1 i ■ m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 25.40 25.60 25.80 26.00

8481.D GCMS0412.M Wed Apr 17 09:49:13 2002 Page 9

NYC-WTC_000048596

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NYC-WTC_000048596Source: NYC Law Department, mirrored locally

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