GCMS calibration table and instrument parameters, Apr 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\APR1202\8481.D Vial: 26 Acq On : 16 Apr 2002 9:08 am Operator: Sample : gc/ms scan 4/10 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 8 Tridecane Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T. 17.68 0.43 ug/1 84546 Naphthalene-d8 15.87

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Tridecane 184 C13H28 000629-50-5/93/ 2 Hexadecane 226 C16H34 000544-76-3 91 3 Heptadecane 240 C17H36 000629-78-7 91 4 Tetradecane 198 C14H30 000629-59-4 91 Abundance Scan 1376 (17.675 min): 8481.D (-) m/ z 57.00 100.00% 57 43

71 5000 85 > 1 * F Fph FT 1 1 ' 1 7I 1 1 ' TT 99 113 126 141 184 17.40 17.60 17.80 18.00 - Tu" T r I I I ! | I I ! I r r — > | I ! I I — I I I | I I 1 1 | I ! ! I | I r m/ z 43.05 80.31%| m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 Abundance #18989: Tridecane 57 43

71 ,_____ / 5000 85 TTTFTTTTTr TTTPP 17.40 17.60 17.80 18.00 m/ Z 71.10 56.81%| 1 99 112 127 141 184 ■ ■ i 1 1 ' ■ 1 1 1 1 1 1 1 1n—I 1-1 m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 Abundance #70787: Hexadecane 43 57 A4A-----AATA 71 17.40 17.60 17.80 18.00 5000 m/ z 85.00 35.75% 85

27 , I I i ' ■ ■ ■ i 1 ■ I 1 1 1 1 1 99 113 127 141 155 226 m/z—> 20 40 60 80 100 120 140 160 180 200 220 240 Abundance #71191: Heptadecane ■ ' i 1 — , AM, A. 57 17.40 17.60 17.80 18.00 43 m/z 41.05 35.44 71 5000 85

। -। ■ I1 1 1 1 II +—r ' 99 'I ■ 1 113 127 141 | 1 | ' | ■ 1 | ■ 1 1 1 | > । 1 1 | । > 240 m/z-> 20 40 I60 80 100 120 140 160 180 200 220 240 17.40 17.60 17.80 18.00

8481.D GCMS0412.M Wed Apr 17 09:49:12 2002 Page 8

NYC-WTC_000048595