GCMS analysis results for sample AE01503, Mar 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\FEB2102\1503.D Vial: 26 Acq On : 22 Feb 2002 4:46 pm Operator: Sample : gc/ms scan 1/22 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 6 Hexadecane Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T.

29.09 0.23 ug/1 20100 Phenanthrene-dlO 25.74

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Hexade cne 226 C16H34 000544-76-3 38 2 Heptadecane 240 C17H36 000629-78-7 23 3 l-Pentanol, 4-methyl-2-propyl- 144 C9H20O 054004-41-0 23 4 Tridecane 184 C13H28 000629-50-5 .05 100.00% 23 Abundance Scan 2619 (29.089 min): 1503.D (-) m/ z 43 43 57 71 5000 85 99 . 111 28.80 29.00 29.20 29.40 ■ ' i ' ■

------ i ' ■ ' ■ 1 1 m/z 57.00 94.01% m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 Abundance #70789: Hexadecane 43 57

71 5000 28.80 29.00 29.20 29.40 85 m/ z 71.00 67.07%

M ■ I

l 1 ■ ■ ■ i ' ■ I i' 1 ■ 11'-" 99,113 127 .................... ...... . ......... m/z->___ 20 40__ 60 80 100 120 140 160 180 200 220 240 Abundance *1:01 Heptadecan 43 57 W) MA, 71 28.80 29.00 29.20 29.40 5000 m/ z 84.95 35.81% 85

m/z-> Abundance 20 i ■ ■ ■ ■ । 40 ■ .... 99 113 127 141 60 .. 80__ 100__ 120. 140__ 160__ 180 F7 #8543:1 -Pentanol, 4-methyl-2-propyl- 200 220 240 240 aAn/Mamuar 28.80 29.00 29.20 29.40 m/z 42.15 28.38% 71 5000 27 83

m/z—> 20 1.4 I ■ ' ' ' 1 1 ‘ 40 , 1 II 98 111 126 1 1 i ' ■ > j > ■ 60 80 100 120 140 160 180 200 220 240 28.80 29.00 29.20 29.40

1503.D GCMS0208.M Tue Feb 26 15:12:59 2002 Page 6

NYC-WTC_000003603