GCMS analysis results for sample AE01462, Feb 2002

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Data File : C:\HPCHEM\1\DATA\FEB2102\1462.D Vial: 15 Acq On : 22 Feb 2002 3:53 am Operator: Sample : gc/ms scan 1/22 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 7 Octadecane Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

25.39 0.57 ug/1 70656 Phenanthrene-dl0 25.74

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Octadecane 254 C18H38 000593-45-3 (97 2 Nonadecane 268 C19H40 000629-92-5 70 3 Tetracosane 338 C24H50 000646-31-1 62 4 Pentacosane 352 C25H52 000629-99-2 62 Abundance Scan 2216 (25.390 min): 1462.D (-) m/z 57.00 100.00% 43 57 71

5000 85 192 -& 4144 4_ PM_ I — I Yr AP P A I 99. 25.00 25.20 25.40 25.60 25.80

miz-? 40 60 441127.146160, 254 m/z ' 1 1 1 1 * I 1 1 1 1 1 1 ‘ 11 1 1 ' 1 1 I ' 1 1 1 I 1 1 1 1 I1 ' 1 ’ 1 1 80 100 120 140 160 180 200 220 240 260 280 300 320 340 43.05 79.90% Abundance #71560: Octadecane 43 57

71 5000 85 25.00 25.20 2540 25.60 25.80 m/z 71.05 69.15% ■ ■ i * ■ . .. ,,. J | 113127141 169183197 254 m/z~> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance 57 43 71 MA -A A I AA । pa. 25.00 25.20 25.40 25.60 25.80 85 5000- m/z 85.05 48.77%

89 113127 183197 268 m/z-> Abundance 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 #73543: Tetracosane MA— • i > ■ ■ ■ । ■ A A ■ > ■ । ■ > ■ • । ■ 43 57 25.00 25.20 25.40 25.60 25.80 71 m/ z 41.05 39.35% 5000 85

99. ll 113127 155169183197 294 338 MA MEAMAAA, w Ar ' 'i TITTI—"u-g TT । TIr ■ i ■ ■1111 ■ ■111'■■i’■■’i1111111'1111'11111 '11 miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 25.00 25.20 25.40 25.60 25.80

1462.D GCMS0308.M Mon Mar 25 08:27:43 2002 Page 7

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