GCMS analysis results for sample AE01462, Feb 2002

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Data File : C:\HPCHEM\l\DATA\FEB2102\1462.D Vial: 15 Acq On : 22 Feb 2002 3:53 am Operator: Sample : gc/ms scan 1/22 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 8 1-Hexadecanol Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

28.98 0.59 ug/1 73304 Phenanthrene-dl0 25.74

Hit# of 5 Tentative ID MW MolForm CAS# Qu.

1 1-Hexadecanol 242 C16H340 036653-82-4 2 1-Hexacosanol 382 C26H540 000506-52-5 58 3 1-Tetracosanol 354 C24H50O 000506-51-4 58 4 1-Octadecene 252 C18H36 000112-88-9 49 Abundance Scan 2607 (28.979 min): 1462.D (-) ] m/z 83.0.5 100.00% 55 63

5000 111 AAA

+2s. 1 1 ■ ■ i ■ ■ ■ ■ । 1 1 > ■ 1 > 31 28.60 28.80 29.00 29.20 29.40 — "‘I i ■ ■ ■ • i • ■ ■ ■ i ■ ■ ■ ■ i ■ ■ > ■ i ■1 i11111 m/z 54.95 98.27% m/z-2 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #32424' i-Hexadecanoi 55 83

5000 28.60 28.80 29.00 29.20 29.40 111 m/z 69.00 91.96% ■ 1 196 224 1 1 r 1 I ' 1 ' T ■'11 ■ ■ 1 r ; 1' i'1 “ i1 ‘111'11111111111111111 ‘ i11111 ‘1111111111111 r1111 m/Z“>_____ 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance 43

28.60 28.80 29.00 29.20 29.40 5000 83 m/z 43.00 89.62% 68 111 ....... —........................................... ................................................ 336 364 m/z~> _ 40. 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #49775: 1-Tetracosanol 43 28.60 28.80 29.00 29.20 29.40 m/ z 57.00 81.54% 5000- 83

TT-p-r-rTp- 68 -_ 111 ................................................ "Tt’11711111110111TETEETTTETTTET ’1’’1IIIIVB 308—O—IITUIIIITT 336 W m/z~> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 28.60 28.80 29.00 29.20 29.40

1462.D GCMS0308.M Mon Mar 25 08:27:47 2002 Page 8

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