GCMS analysis results for sample AE01462, Feb 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\FEB2102\1462.D Vial: 15 Acq On : 22 Feb 2002 3:53 am Operator: Sample : gc/ms scan 1/22 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 9 1-Octadecene Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

31.31 15.24 ug/1 1566990 Chrysene-dl2 33.81

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Octadecene 252 C18H36 000112-88-9 95 2 Phosphonic acid, dioctadecyl ester 587 C36H75O3P 019047-85-9 93 3 5-Eicosene, (E)- 280 C20H40 074685-30-6 70 4 1-Octadecanol 270 C18H380 000112-92-5 70 Abundance 1Scan 2861 (31.311 min): 1462.D (-) | m/z 55.00 1.00.00% 55

5000- 83 4 69 97 113127 ■ ■ l 1 1 ■ - j ■ r 1 • I

, , .III, , | _ ,|, J,. 141155 169 183 197 211225 239252 267 281 295 31.00 31.2031 40 31 60 324 — TTT"TTTTTTTTT । m/Z 43.00 50.53% m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #71503: 1-Octadecene 1 55

5000- 70 83 „ ! 97 ■ ■ l • ■ A____ ■ ■ ■ l > . 1 . I . . 1 ■ I 31.00 31.20 31.40 31.60 42 m/ Z 83.05 45.61% ! 125 TIgr I, 252 In’III———111IITTrTTEII1111"’11’1111IO"IIIIIITOIIITTT m/z->_ ^0 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance 55 69 83 ...... — =...... ===== 97 31.00 31.20 31.40 31.60 5000 m/ z 73.00 45.15% 111 42 136 1 ■ ।111 ■ p m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #39520: 5-Eicosene, (E> ...... > । I ■> 1 1 I 1... 'i i । 3 ....... । । 55 31.00 31.20 31.40 31.60 83 m/ z 57.0,0 43.81% 97 5000 70 111

It 125,39 II l 252 280 —.......... 7.......................... , ' ' I 1 ' 1 1 I ' 1 ( ' I m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 | 31.00 31.20 31.40 31.60

1462.D GCMS0308.M Mon Mar 25 08:27:52 2002 Page 9

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