GCMS results for sample AE10064, May 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\1\DATA\MAYO 302\10064.D Vial: 37 Acq On 5 May 2002 3:18 am Operator: Sample GC/MS SCAN 4/26 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 1-Octadecene Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 31.16 7.95 ug/1 497743 Chrysene-dl2 33.63 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Octadecene 252 C18H36 000112-88-91 91 2 1-Docosene 308 C22H44 001599-67-3 76 3 Phosphonic acid, dioctadecyl ester 587 C36H75O3P 019047-85-9 76 4 5-Eicosene, (E)- 280 C20H40 074685-30-6 76 Abundance Scan 2850(31.160 min): 10064. D (-) m/z 55.10 100.00% 55

5000 4' 73 97 _________ / ।l1■ ' 1 । 1 ■ T ■ i 11''1’1 I’ 111 127 30,80 31,00 31.20 31.40 , I, Ji al 141155169183197211 225 252 295 TTIT r ‘ I ■ 1 ' ‘ i 1 1 1 1 I ' 1 1 1 I 1 1 m/ z 43.05 56.33% m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #71503:1-Octadecene 55

83 97 5000 70 30.80 31.00 31.20 31.40 42 111 m/z 57.10 49.98% 125 ' ■ i' 1 1 1 1 ■ 1 1 I,.............................................. 252.................... m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #72943:1-Docosene 55 1 .. 83 97 30.80 31.00 31.20 31,40 5000 m/z 73.10 45.98% 70 111 42 125 ’ I’1 i ■ 11 ■ i1 1139 .....................................308 I'11 ’ I''''I'''‘111111''1111 * 1'111 11111 111' 1 111 1 ’' 111' mz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #60683: Phosphonic acid, dioctadecyl ester 9. ) 111111 55 69 83 30.80 31.00 31.20 31.40 97 m/z 69.00 41.95%|

5000 111 42 136 ■ ■ i ■ ' "IT 1 1 i 1 , , | , 1 I, , 1 ........ ''11' ‘111'''11'''‘11'11111111'''11''111111111111111111111' 1 jm - 10 . । , । , , , . । , m/z—> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 30,80 31,00 31,20 31.40

10064.D GCMS0501.M Tue May 07 12:00:49 2002 Page 4

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