GCMS calibration data for TCLP method, May 2002

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GCMS calibration table and instrument data for TCLP analysis recorded on May 5-7, 2002.

NYC-WTC_000022953–000022960

Folder label: “GCMS X 5/8/02 A 5/10/02”

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« Quantitation Report (QT Reviewed) 3 Data File C:\HPCHEM\1\DATA\MAY0 302\9569.D Vial: 43 Acq On 5 May 2002 9:10 am Operator: Sample GC/MS SCAN 4/23 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 7 14:48 2002 Quant Results File: GCMS0501.RES

Quant Method Title Last Update Response via : : : : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) 209 625/TCLP calibration table Wed May 01 10:40:31 2002 Initial Calibration QV8 p )

DataAcq Meth : GCMS0501

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 12.19 152 501520 40.00 ug/1 -0.02 10) Naphthalene-d8 15.82 136 1844680 40.00 ug/1 -0.03 17) Acenaphthene-diO 21.14 164 986751 40.00 ug/1 -0.01 30) Phenanthrene-diO 25.57 188 1397585 40.00 ug/1 -0.02 38) Chrysene-dl2 33.64 240 922465 40.00 ug/1 -0.03 44) Perylene-dl2 37.87 264 638322 40.00 ug/1 -0.01

System Monitoring Compounds 28) TCMX 23.27 209 30950 6.44 ug/L -0.02 Spiked Amount 10.000 Recovery = 64.40% Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,21 -oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.89 128 218 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 22) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 22.61 149 901 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 29) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D. 31) N-Nitrosodiphenylamine 0.00 168 0 N.D. 32) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 3 3) Hexachiorobenzene 0.00 284 0 N.D. 34) Phenanthrene 25.58 178 248 N.D. (#) = qualifier out of range (m) = manual integration 9569.D GCMS0501.M Tue May 07 14:48:36 2002 Page 1

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GCMS calibration data for TCLP method, May 2002 · Box DEP Box 18

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GCMS calibration table and instrument data for TCLP analysis recorded on May 5-7, 2002.

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