GCMS calibration data for TCLP analysis, May 2002

Machine-extracted title · confidence 90%

Calibration table listing response factors for deuterated standards used in TCLP analysis on May 5, 2002.

NYC-WTC_000023195–000023202

Folder label: “GCMS X 5/8/02 A 5/9/02”

Page image

OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

A Data File C:\HPCHEM\1\DATA\MAY0 302\9577.D Vial: 50 Acq On 5 May 2002 4:02 pm Operator: Sample GC/MS SCAN 4/23 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 7 14:56 2002 Quant Results File: GCMS0501.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed May 01 10:40:31 2002 Response via : Initial Calibration DataAcq Meth : GCMS0501

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.20 152 453543 40.00 ug/1 -0.02 10) Naphthalene-d8 15.82 136 1650151 40.00 ug/1 -0.03 17) Acenaphthene-diO 21.13 164 885597 40.00 ug/1 -0.02 30) Phenanthrene-diO 25.57 188 1220287 40.00 ug/1 -0.02 38) Chrysene-dl2 33.63 240 777592 40.00 ug/1 -0.04 44) Perylene-dl2 37.86 264 519970 40.00 ug/1 -0.02

System Monitoring Compounds 28) TCMX 23.27 209 15774 3.66 ug/L -0.02 Spiked Amount 10.000 Recovery = 36.60%

Target Compounds 2) N-nitroso-dimethyl amine 3) bis(2-Chloroethyl)ether 4) 1,3-Dichlorobenzene 5) 1,4-Dichlorobenzene 6) 1,2-Dichlorobenzene 7) 2,21-oxybis(1-Chloropropan 8) N-Nitroso-di-n-propylamine 9) Hexachloroethane 11) Nitrobenzene 12) Isophorone 13) bis(2-Chloroethoxy)methane 14) 1,2,4-Trichlorobenzene 15) Naphthalene 16) Hexachlorobutadiene 18) Hexachlorocyclopentadiene 19) 2-Chloronaphthalene 20) Dimethylphthalate 21) 2,6-Dinitrotoluene 22) Acenaphthylene 23) Acenaphthene 24) 2,4-Dinitrotoluene 25) Diethylphthalate 26) 4-Chlorophenyl-phenylether 27) Fluorene 29) Azobenzen/ 1,2-Diphenylhyd 31) N-Nitrosodiphenylamine 32) 4-Bromophenyl-phenylether 33) Hexachlorobenzene 3 4) Phenanthrene (#) = qualifier 9577.D GCMS0501.M Qvalue 0.00 74 0 N.D. 0.00 93 0 N.D. 0.00 146 0 N.D. 0.00 146 0 N.D. 0.00 146 0 N.D. 0.00 45 0 N.D. 0.00 70 0 N.D. 0.00 117 0 N.D. 0.00 77 0 N.D. 14.53 82 3378 N.D. 15.21 93 279 N.D. 0.00 180 0 N.D. 15.88 128 793 N.D. 0.00 225 0 N.D. 0.00 237 0 N.D. 0.00 162 0 N.D. 20.48 163 454 N.D. 0.00 165 0 N.D. 0.00 152 0 N.D. 0.00 153 0 N.D. 0.00 165 0 N.D. 22.61 149 1129 N.D. 0.00 204 0 N.D. 0.00 166 0 N.D. 0.00 77 0 N.D. 0.00 168 0 N.D. 0.00 248 0 N.D. 0.00 284 0 N.D. 25.64 178 572 N.D. out of range (m) = manual integration Tue May 07 14:57:19 2002 Page 1

NYC-WTC_000023195

OCR can misread numbers and units. Confirm readings against the page image before using them.

NYC-WTC_000023195Source: NYC Law Department, mirrored locally

Related records

Browse subjects →

Ranked by indexed similarity. Reasons describe shared subjects and filing context; check the source records.

Same-box records

GCMS calibration data for TCLP method, May 2002 · Box DEP Box 18

NYC-WTC_000022953

GCMS calibration table and instrument data for TCLP analysis recorded on May 5-7, 2002.

1 shared topics · Same agency, volume and box · similarity 0.999