NYC-WTC_000022953
GCMS calibration table and instrument data for TCLP analysis recorded on May 5-7, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗Document / 8 pages
GCMS calibration data for TCLP analysis, May 2002
Machine-extracted title · confidence 90%Calibration table listing response factors for deuterated standards used in TCLP analysis on May 5, 2002.
NYC-WTC_000023195–000023202Folder label: “GCMS X 5/8/02 A 5/9/02”
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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)
A Data File C:\HPCHEM\1\DATA\MAY0 302\9577.D Vial: 50 Acq On 5 May 2002 4:02 pm Operator: Sample GC/MS SCAN 4/23 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 7 14:56 2002 Quant Results File: GCMS0501.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed May 01 10:40:31 2002 Response via : Initial Calibration DataAcq Meth : GCMS0501
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 12.20 152 453543 40.00 ug/1 -0.02 10) Naphthalene-d8 15.82 136 1650151 40.00 ug/1 -0.03 17) Acenaphthene-diO 21.13 164 885597 40.00 ug/1 -0.02 30) Phenanthrene-diO 25.57 188 1220287 40.00 ug/1 -0.02 38) Chrysene-dl2 33.63 240 777592 40.00 ug/1 -0.04 44) Perylene-dl2 37.86 264 519970 40.00 ug/1 -0.02
System Monitoring Compounds 28) TCMX 23.27 209 15774 3.66 ug/L -0.02 Spiked Amount 10.000 Recovery = 36.60%
Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,21-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) Isophorone 14.53 82 3378 N.D. 13) bis(2-Chloroethoxy)methane 15.21 93 279 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.88 128 793 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 20.48 163 454 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 22) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 22.61 149 1129 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 29) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D. 31) N-Nitrosodiphenylamine 0.00 168 0 N.D. 32) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 33) Hexachlorobenzene 0.00 284 0 N.D. 3 4) Phenanthrene 25.64 178 572 N.D. (#) = qualifier out of range (m) = manual integration 9577.D GCMS0501.M Tue May 07 14:57:19 2002 Page 1
NYC-WTC_000023195
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