GCMS analysis results for sample AE01503, Mar 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\FEB2102\1503.D Vial: 26 Acq On : 22 Feb 2002 4:46 pm Operator: Sample : gc/ms scan 1/22 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 7 1-Octadecene Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

31.31 3.79 ug/1 253680 Chrysene-dl2 33.80

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Octadecene 252 C18H36 000112-88-91 2 Phosphonic acid, dioctadecyl ester 587 C36H75O3P 019047-85-9 93 3 1-Octadecanol 270 C18H380 000112-92-5 76 4 l-Docosene 308 C22H44 001599-67-3 76 Abundance Scan 2861 (31.310 min): 1503.D (-) m/ z 55.00 100.00% 55

43 5000 69 83 97 i । 111 127 31.00 31.20 31.40 31.60 —— .1 ' lli il . ."I'l , al 139151 167179 207 239252____ 295 1,11 1 '1 I ''1' I n ' 'T' ' ' ' 1 ' ' ' I ' '' ■I ' ' ‘'I ' ' ' ' 1 1 1 1 ' 1 1 1 ' 1 1 1 1 1 1 1 1 m/ z 43.00 50.71% m/z-2 40 60 80. 100. 120. 140 160 180 200 220 240 260 280 300 Abundance #71503:1 -Octadecene

55 83 97 5000 70 31.00 31.20 31.40 31.60 111 i 42 m/ z 57.00 46.34% . I ' T'T * ‘ | * 125 , J , y................................................ 252................... m/z->40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance Te83 Pheschond 00, dioctadacyi ester 43 55 69 83 - . _- _ ___ - J A 97 31.00 31.20 31.40 31.60 ‘ 5000 m/z 83.00 45.75% 111 136

m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #72029:1-Octadecanol —"! ' 1 ' ' I 43 55 69 83 31.00 31.20 31.40 31.60 97 m/ z 73.00 44.35% 5000 111 125 || | | 224 252 V ■ ■ i ■ ' ’TT T-r-p m/z-> 40 60 80 .100 120 140 160 180 200 220 240 260 280 300 31.00 31.20 31.40 31.60

1503.D GCMS0208.M Tue Feb 26 15:13:04 2002 Page 7

NYC-WTC_000003604