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GCMS analysis results for sample AE01503, Mar 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE01503 conducted on March 6, 2002.

NYC-WTC_000003591–000003606

Folder label: “GCMS X 1/23/02 A 2/22/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\FEB2102\1503.D Vial: 26 Acq On : 22 Feb 2002 4:46 pm Operator: Sample : gc/ms scan 1/22 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 8 Decanedioic acid, bis(2-ethylh Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

36.28 4.06 ug/1 208726 Perylene-dl2 38.08

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Decanedioic acid, bis(2-ethylhexyl) 426 C26H50O4 000122-62-3(87 2 Propanedioic acid, hexyl-, diethyl 244 C13H2404 005398-10-7 25 3 2-Undecene, 4,5-dimethyl-, [R@,S@-( 182 C13H26 055170-93-9 16 4 1-Decene, 3,4-dimethyl- 168 C12H24 _ 050871-03-9 12 Abundance Scan 3402 (36.277 min): 1503.D (-) m/z 185.10 100.00% 185

57 5000 70 43 , — 7

125 143 166 203 297 315 36.00 36.20 36.40 36.60 .I t L , .J l .. pt 1 253 Tr m/z 57.00 50.43% m/z- 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #55661: Decanedioic acid, bis(2-ethylhexyl) ester 185

5000 57 71 112 36.00 36.20 36.40 36.60 ! 84 98 m/z 70.10 38.86% • ' I > ■ >| ........ i ] . .: ■ । . . . , । , | 125 143 166 : 203 298 316 _ _____________ _ _________ 120 140 160 180 200 220 240 260 280 300 320 Abundance ........ 25 57 70 ... p r, 36.00 36.20 36.40 36.60 5000- 83 112 m/z 71.05 36.94%

42 ■ ■ i' ■ ■ ■ i ■ :...... 98................ 199 217 m/z-> 40 60 JO 100 120 140 160 180 200 220 240_260_280300 320 Abundance ~ #18485:2-Undecene, 4,5-dimethyl-, [R@,S@-(Z)]- ‘ I‘ ' 1 I ' 1 1 1 I ' 1 43 57 36.00 36.20 36.40 36.60 71 m/z 55.00 33.40% 5000

98 112

’ I’* -IB 44 ■ ■ i1' ■ li ■ ■ 140 ......... 182.................................... T-p-r m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 36.00 36.20 36.40 36.60

1503.D GCMS0208.M Tue Feb 26 15:13:09 2002 Page 8

NYC-WTC_000003605

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NYC-WTC_000003605Source: NYC Law Department, mirrored locally

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