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GCMS comments for sample AD29521, Jan 2002

Machine-extracted title · confidence 95%

Laboratory commentary confirming no unusual compounds detected in sample AD29521 during GCMS scan on January 4, 2002.

NYC-WTC_000036530–000036541

Folder label: “GCMS X 12/6/01 A 12/12/01 - 12/13/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC1301\29521.D Vial: 8 Acq On : 13 Dec 2001 4:42 pm Operator: 209 GALOS Sample : gems scan 12/6 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 4 Decanedioic acid, bis(2-ethylh Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

35.56 0.65 ug/1 154754 Perylene-dl2 37.10

Hit# of 5 Tentative ID MW MolForm CAS# Qual 000122-62-3 90) 1 Decanedioic acid, bis(2-ethylhexyl) 426 C26H50O4 2 Propanedioic acid, hexyl-, diethyl 244 C13H2404 005398-10-7 27 3 2-Undecene, 4,5-dimethyl-, [R@,S@-( 182 C13H26 055170-93-9 17 4 2-Undecene, 2,5-dimethyl- 182 C13H26 049622-16-4 16 Abundance Scan 3324 (35.562 min): 29521.D (-) m/z 185.10 100.00% 185 57 5000 41 112 83 • i ■ ■ • • i

m/z-> —LAL, 40 60 143 166 - 221 253 281 297 TTmpr 355 I *'4 ' I TT 80 100 120 140 160 180 200 220 240 260 280 300 320 340 m/z 35.20 35.40 35.60 35.80 57.00 64.92% 'Abundance #55661: Decanedioic acid, bis(2-ethylhexyl) ester 185

5000- 57 —94 TT 112 35.20 35.40 35.60 35.80 m/ z 70.00 45.20% UuX 83 1

C 143 166 298 316 — TTTIPT '203 I"•'I'"'I IT I ’' •' I' " ’ I' TT m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 'Abundance #32687: Propanedioic acid, hexyl-, diethyl ester 57 TT 35.20 35.40 35.60 35.80 5000 112 m/z 71.00 40.32% 83 42 ■i t l 199 217 m/z-> 40 60 80 100120 140 160 180 200 220 240 260 280 300 320 340 .............. Abundance #18485: 2-Undecene, 4,5-dimethyl-, [R@,S@-(Z)]- AM AA 'I1 4444 —WA A 57 35.20 35.40 35.60 35.80 m/z 55.00 38.38% 5000

J 112 140 m/z-> ■11''' ■ r 40 60 48083H . —.... 183 T’TTII’ . . i । . • i » । r i i . । . . . i । » I • . । ( i • < । i i < i j . 100 120 140 160 180 200 220 240 260 280 300 320 340 ‘IT 35.20 35.40 35.60 35.80 . . p । > ij r .> , ।

29521.D GCMS1126.M Fri Dec 21 13:15:34 2001 Page 4

NYC-WTC_000036540

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NYC-WTC_000036540Source: NYC Law Department, mirrored locally

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