GCMS analysis results for sample AD29187, Jan 2002

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Laboratory report documenting GCMS analysis of sample AD29187 conducted on January 4, 2002, by the DEP.

NYC-WTC_000037116–000037125

Folder label: “GCMS X 12/10/01 A 12/15/01”

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NYC 9/11 Public Portal Document

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Data File : C:\HPCHEM\1\DATA\DEC1401\29187.D • Vial: 19 Acq On : 15 Dec 2001 8:05 pm Operator: 209 GALOS Sample : gems scan 12/10 a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 2 Decanedioic acid, bis(2-ethylh Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

35.57 0.82 ug/1 153258 Perylene-dl2 37.10

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Decanedioic id, bis(2-ethylhexyl) 426 C26H50O4 000122-62-3 50 2 Propanedioi acid, hexyl-, diethyl 244 C13H2404 005398-10-7 38 3 Benzene, -nitro-2-(octyloxy)- 251 C14H21NO3 037682-29-4 32 4 Cyclopr pane, 1-(2-methylbutyl)-1-( 168 C12H24 064723-36-0 27 'Abundance Scan 3325 (35.566 min): 29187.D (-) m/z 185.10 100.00% 185 57 5000 70 43 83 112 , | 98 125139 157 240253 283 315 35.20 35.40 35.60 35.80 । ■11 • ■ 4 +4 * 1"IT11 J nr I- u h a 209 i ' ■ ■ ' i Tnpurr m/z 57.00 62.08% mz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #55661: Decanedioic acid, bis(2-ethylhexyl) ester 185

5000 57 iT 71 112 35.20 35.40 35.60 35.80 m/ z 70.00 44.40%

m/z-> ......... — 40 60 23 ' I 1' ' 'I 80 125 143 166 TTPTTT 203 100 120 140 160 180 200 220 240 260 280 300 320 Tuunugm*i 298 316 I " "I...........

Abundance #32687: Propanedioic acid, hexyl-, diethyl ester 57 70 35.20 35.40 35.60 35.80______

7 5000- 83 ”2

m/z--> 42 ■11 ■ ■ 40 91 ll 11 • ■ i ■ • ■ ■ i ■ ■ ■ ■ i ■ ■ 60 80 100 199 217 'i'111i1111।1 • 11।1 • 1 1 । 1 • ■ 1 । • 1 • • । * 120 140 160 180 200 220 240 260 280 300 320 Abundance #34102: Benzene, 1-nitro-2-(octyloxy)- 57

J 35.20 35.40 35.60 35.80_______ m/z 71.10 37.40% 71 5000 112 84 139

■ ■ i • ■ i ■' • ’ i 97 ,ii J 221 251 T Ter T ' 1 ' 'I ' ' ' ' I ■ ' ' ■ i ' ' ' ' i ' ' ' ~i ' ' ' ■ i ' ' '■ 1 i ' ‘ ' i ' । । 1 1 1 11 । I ' M/ , , AL m/z—> 40 60 80 100 -120 140 160 180 200 220 240 260 280 300 320 35.20 35.40 35.60 35.80

29187.D GCMS1126.M Fri Dec 28 13:07:32 2001 Page 2

NYC-WTC_000037124

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NYC-WTC_000037124Source: NYC Law Department, mirrored locally

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