GCMS sample analysis report, Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C: \HPCHEM\ 1 \DATA\JAN1 802\31500.D Vial: 13 Acq On : 19 Jan 2002 3:19 am Operator: 209 GALOS Sample : gc/ms scan 12/31 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 3 Decanedioic acid, bis(2-ethylh Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

35.39 2.97 ug/1 464847 Perylene-dl2 36.86

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Decanedioic acid, bis(2-ethylhexyl) 426 C26H50O4 000122-62-3 64 2 Nonane,/3-methyl- 142 C10H22 005911-04-6 25 3 Propanedioic acid, hexyl-, diethyl 244 C13H2404 005398-10-7 25 4 Octane, 1,1‘-oxybis- Abundance ; 57 Scan 3305 (35.385 min): 31500.D (-) ” 185 242 C16H340 ' m/z "T ' 000629-82-3 22

5000 43 70 112 98 35.00 35.20 35.40 35.60 35.80 | 1 —4 139 166 TImu1 ’ 203 268 utunmuuuu 297 315 —uuonur m/z 57.00 66.28% miz 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #55661: Decanedioic acid. bis(2-ethylhexy!) ester 185

5000 57 71 112 35.00 35'20 35.40 35.60 35.80 98 m/z 70.10 46.62% 143 166 203 298 316 ! I ' ‘ ' ' I “ ' 1 I ‘ . ।।. .'i.. ■. । r,t.... j.... j।11. miz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance 48075 Nonane, -methy- 57 43 71 mmm 35.00 35.20 35.40 35.60 35.80 5000 m/z 71.05 42.14% 27 113 85 142 i 1‘TTr1r-trT-"-r111211-33111211-1"11--fTTTT ‘11‘11111321131231——233333S1" m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #32687: Propanedioic acid, hexyl-, diethyl ester AMRffTTTTT 57 35.00 35.20 35.40 35.60 35.80 m/z 55.00 41.53% 5000 83 112

42 98 # | T022t1 199 217 ‘020n1—umuutnd0hImO31 I' “ 11 ‘ * 1 • • miz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 35.00 35.20 35.40 35.60 35.80

31500.D GCMS0103.M Wed Feb 06 15:34:24 2002 Page 3

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