GCMS scan results for sample AD28802 dated December 16, 2001, detecting bis(2-Ethylhexyl)phthalate and other compounds.
NYC-WTC_000035460–000035472Folder label: “GCMS X 11/27/01 A 12/7/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\HPCHEM\1\DATA\DEC0601\28802.D Vial: 29 Acq On 7 Dec 2001 3:00 am Operator: 209 GALOS Sample 11/27 gc/ms scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L
Peak Number 5 Decanedioic acid, bis(2-ethylh Concentration Rank 1
R.T. EstConc Area Relative to ISTD R.T.
35.57 15.95 ug/1 3998370 Perylene-dl2 37.10
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Decanedioic acid, bis(2-ethylhexyl) 426 C26H50O4 000122-62-3 91 2 [1,1'-Biphenyl]-4-ol, 3-amino- 185 C12H11NO> 001134-36-7 32 3 Pyridine, 4-[4-methoxyphenyl]- 185 C12H11NO। 000000-00-0 17 . . 4 Pyridine, 4-[4-methoxyphenyl]- 185 C12H11NO1_____ 000000-00-0 17 Abundance Scan 3325 (35.567 min): 28802.D (-) m/z 185.10 100.00% 185
57 5000-
lse 166 203 221 240 355 268 297 315 35.20 35.40 35.60 35.80 m/ z 57.00 51.77%
L miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 'Abundance #55661: Decanedioic acid, bis(2-ethylhexyl) ester 185
5000 - 57 1 I 1 1 > ■ I ■ 112 35.20 35.40 35.60 35.80 83 m/z 70.00 36.32% 143 166 203 298 316 TTTTT IT . I .’l TT . I T*u i ■ •" i I""I m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #19199: [1.1-Biphenyl]-4-ol, 3-amino- 185
35.20 35.40 35.60 35.80 5000 m/z 71.00 34.99% 156 139 113 J 1 !■ 1 " I" " I' r " ■ i " '' i' TUITITTTTT I TTTIT ' i " '' i'' " I'' " i ■ ■'' i r"'i miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #19197: Pyridine, 4-[4-methoxyphenyl]- 185 35.20 35.40 35.60 35.80 m/z 112.10 30.62% 5000 142 115 170 63 89 I
m/z-> 40 TTp P ■ ■' ■ ir' " i i" • • r •" i •" • i •" • i • •" i" ‘' rrn 1 r' rri 60 80 100 120 140 60 180 200 220 240 260 280 300 320 340 360 ....... ......... ...... 35.20 35.40 35.60 35.80
28802.D GCMS1126.M Wed Dec 12 11:35:04 2001 Page 5
NYC-WTC_000035471
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NYC-WTC_000036311
Laboratory analysis report for sample AD29285 conducted on December 28, 2001, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035831
Lab notes for sample AD29141 indicate detection of bis(2-Ethylhexyl)phthalate and one LCS compound outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035640
Lab report noting bis(2-Ethylhexyl)phthalate detection, recovery issues, and low pH.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035808
Laboratory analysis notes for sample AD29023 indicating no unusual compounds detected in GCMS scan; one of forty-three compounds in quality control standard outside acceptance rang
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036255
Laboratory analysis report for sample AD29294 conducted on December 28, 2001, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036325
Laboratory GCMS analysis report for sample AD29229 conducted on December 28, 2001, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036137
Laboratory report noting GCMS scan results for sample AD29233 with phthalates and nonadecanol detected.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035618
Lab report noting bis(2-Ethylhexyl)phthalate detection and recovery issues in a water sample.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036391
Laboratory report documenting GCMS analysis of sample AD29298 conducted on January 4, 2002, showing unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033580
Laboratory report documenting GCMS analysis of environmental sample AD27771 conducted on January 3, 2002.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033674
Gas chromatography-mass spectrometry analysis of environmental sample AD27826 conducted on January 3, 2002, detecting unknown compounds and 2,4-DDD surrogate standard.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000032160
Laboratory report documenting GCMS analysis of sample AD26827 identifying unknown compounds on December 21, 2001.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000035422
Department of Environmental Protection record logging GCMS X samples from November to December 2001.
Filed in the same folder
NYC-WTC_000035423
Label for a GCMS environmental sample collected between November and December 2001.
Filed in the same folder
NYC-WTC_000035426
Log recording sample volume, drip rates, and addition details for GCMS analysis in December 2001.
Filed in the same folder
NYC-WTC_000035435
Laboratory report of a method blank analyzed on December 16, 2001, showing non-detect results for target compounds.
Filed in the same folder
NYC-WTC_000035439
Calibration data for GCMS analysis of volatile organic compounds dated December 6, 2001.
Filed in the same folder