GCMS method 508 blank results, Dec 16 2001

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Library Search Compound Report

Data File C:\HPCHEM\1\DATA\DECO6O1\LBB.D Vial: 35 Acq On 7 Dec 2001 8:52 am Operator: 209 GALOS Sample 11/28 gc/ms scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Decanedioic acid, bis(2-ethylh Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

35.64 270.05 ug/1 68307800 Perylene-dl2 37.11

Hit# of 5 Tentative ID MW MolForm CAS#

1 Decanedioic acid, bis(2-ethylhexyl) 426 C26H50O4 000122-62-3 2 [1,1 ’-Biphenyl]-4-ol, 3-amino- 185 C12H11NO 001134-36-7 35 3 Pyridine, 4-[4-methoxyphenyl]- 185 C12H11NO 000000-00-0 17 4 Propanedioic acid, hexyl-, diethyl 244 C13H2404 005398-10-7 10

7 (Abundance Scan 3333 (35.640 mln): LBB.D (-) m/z 185. 100.00% 185

57 5000 112 83 35.40 35.60 35.80 36.00 1 miz-? 0- 3 4 414113,66.1,203221240, 268,297315340 369,397.427 40 60 80 100 120140160180 200 220 240 260 280 300 320 340 360 380 400 420 7 m/z 53.90% Abundance #55661: Decanedioic add. bis(2-ethylhexy!) ester 185

5000 57 T-r-p-r 112 35.40 35.60 35.80 36.00 83 m/z 70.00 35.51% | LLLL4166 298316 203 12011310113011221100011——00——30WTTWWUTOImMpuumaa)uW g1 —— rn > J'rm J miz-> 40 60 80 100120140160180200 220 240 260 280 300320340360380400 420 Abundance #19120: [1.1-Biphenyl]-4-of, 3-amino- 185

35.40 35.60 35.80 36.00 5000 m/z 71.00 31.75% ! 156 j 128 _

m/z 70T miz-s 40 60 80100120140180180200220240280280300320340380380400420" Abundance #19196: Pyridine, 4-[4-methoxyphenyl]- —----- - : 185 35.40 35.60 35.80 36.00

5000 115 142 63 89 1 mmmmmmmmmmcmmm — 11111 > 1111 > 111111 —TIP——TT TTPTTr T TI TIT mlz~> 40 60 80 100120140160180200220240260280300 320 340 360380400 420 35.40 35.60 35.80 36.00

LBB.D GCMS1126.M Wed Dec 12 11:23:27 2001 Page 2

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