Laboratory data sheet recording GCMS Method 508 analysis of a blank sample for nitrosamines and chlorinated compounds.
NYC-WTC_000035664–000035673Folder label: “GCMS X 11/28/01 A 12/7/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\HPCHEM\1\DATA\DEC0 6 01\LBB.D Vial: 35 Acq On 7 Dec 2001 8:52 am Operator: 209 GALOS Sanpl e 11/28 gc/ms scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 1-Naphthalenamine, N-phenyl- Concentration Rank 2
R.T. EstConc Area Relative to ISTD R.T.
29.45 2.88 ug/1 828125 Chrysene-dl2 33.01
Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1-Naphthalenamine, N-phenyl- 219 C16H13N 000090-30-2 72 2 4-Benzylquinoline 219 C16H13N 005632-14-4 50 3 Quinoline 6-methyl-2-phenyl- 219 C16H13N 027356-46-3 43 4 1,4-Methanonaphthalene, 1,4-dihydro 218 C17H14 055028-73-4 41 Abundance Scan 2659 (29.452 mln): LBB.D (-) m/z 219.0 100.00% 29
5000 108
63 7 86 95 mtmmmpmmmmmpn 29.20 29.40 29.60 29.80 T39n i -H51mmrin 1, 127 140 153 165 176 189 204 ! TT m/z 218.0 63.74% miz-> 30 40 50 60 70 80 90 100110120130140150160170180190200210220 Abundance #27419: 1-Naphthalenamine, N-phenyl- 219
5000 29.20 29.40 29.60 29.80 108 m/z 217.0 51.20% 85 95 J | 127136 168 188 204 ICm TT TTIUTgeT ‘I’T miz-> 30 40 50 60 70 80 90 100110120130140150160170180190200210220 Abundance ' #27416:4-Benzylquinoline 219 29.20 29.40 29.60 29.80 5000 m/z 108.50 32.35% . 204 91 189 . ‘T TOpppggTg Tor' Ir” /1 TIMgr TTTT TT TTTI miz->___ 30 40 50 60 70 80 90 100110120130140150160170180190200210220 Abundance ' #27409: Quinoline, 6-methyl-2-phenyl- 219 A— 29.20 29.40 29.60 29.80 m/z 220.0 17.19% 5000
94 10S __ 204 66 85 m/z—> TUTT । < 11TTTTDTTTDTTT J". ... .. .... . 30 40 50 60 70 80 90 100110120130140150160170180190200210220 -rm-r 29.20 29.40 29.60 29.80
LBB.D GCMS1126.M Wed Dec 12 11:23:23 2001 Page 1
NYC-WTC_000035670
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NYC-WTC_000035563
GCMS analysis results for sample AD28903 dated December 15, 2001, showing non-detect levels for various compounds.
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Laboratory report of a method blank analysis for sample AD28263 conducted on November 26, 2001.
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Laboratory notes indicating re-extraction is required due to low recovery and potential contamination.
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Laboratory notes identifying potential laboratory contamination by specific esters in sample AD28899.
1 shared topics · Same agency, volume and box · similarity 0.994
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Lab report noting bis(2-Ethylhexyl) Sebacate detection and potential laboratory contamination in a water sample.
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Reference analysis results for target analytes used to verify GCMS instrument performance in December 2001.
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Technical form recording method parameters, drip rates, and analytical data for GCMS testing procedures.
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Laboratory analysis report for sample AD29294 conducted on December 28, 2001, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.993
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Laboratory report noting detection of bis(2-Ethylhexyl)phthalate in sample AD29028 analyzed on December 18, 2001.
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Log recording sample volume, drip rates, and addition details for GCMS analysis in December 2001.
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Lab notes for sample AD29024 indicate detection of bis(2-Ethylhexyl)phthalate and no unusual compounds.
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Method blank report confirming absence of contamination during volatile organic compound testing procedures in January 2002.
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NYC-WTC_000035662
Department of Environmental Protection record logging GCMS X samples from November to December 2001.
Filed in the same folder
NYC-WTC_000035663
Fragmented document containing method 508 data and sample IDs processed by GCMS in late 2001.
Filed in the same folder
NYC-WTC_000035674
Calibration data sheet verifying instrument response for nitrosamines and benzene derivatives.
Filed in the same folder
NYC-WTC_000035678
Document containing calculated reference values for various organic compounds analyzed by GCMS.
Filed in the same folder
NYC-WTC_000035683
Laboratory notes stating the GCMS scan of sample AD28898 revealed no unusual compounds.
Filed in the same folder