GCMS analysis results for sample AE12538, June 2002

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Laboratory report documenting GCMS analysis of sample AE12538 conducted on June 7, 2002, including surrogate recovery data.

NYC-WTC_000014660–000014669

Folder label: “GCMS X 5/28/02 A 6/4/02”

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NYC 9/11 Public Portal Document

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Data File C:\HPCHEM\l\DATA\JUN0302\12538.D Vial: 19 Acq On 4 Jun 2002 2:57 am Operator: Sample gc/ms scan 5/28 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0531.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C: \DATABASE\NBS7 5K. L ********************************************************************* Peak Number 2 Phenanthrene-diO Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 25.57 0.55 ug/1 47127 Phenanthrene-dl0 25.43 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Phenanthrene- diO 188 C14D10 001517-22-2 3 2 2-Quinolin arboxaldehyde, 8-hydrox 188 C10H8N2O2 005603-22-5 3 4H-Pyridol ,2-a] pyrimidin-4-one. 3- 188 C11H12N2O 057773-19-0 42 4 Naphthalene, 1,7 -dimethoxy- 188 C12H1202 005309-18-2 40 Abundance 7 Scan 2235 (25.566 min): 12538.D (-) m/z 188.10 100.00% 1118

5000

' i ■ ■ ' • i •7 ■ r i ■ ■ ■ ■ i ■ • ■ ' i • 80 49 66 92 158 2520 25.40 25.60 25.80 L‘- “ " I " ‘' I ‘1 ■ ■ I' ■'111" 11111 ‘ 11 -HT 1 80.00 14.91% n/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19958: Phenanthrene-d10 1118

5000 ' I ' * ‘ ' I n T I 1 । । ' I ' ‘ 1 ‘ 1 ‘ 25.20 25.40 25.60 25.80 80 m/z 189.10 11.27% 94 160

m/z—> 66 1PPIPRTD 40 50 60 70 - 80 90 100 110 120 130 140 150 160 170 180 190 l Abundance #69165:2-Quinolinecarboxaldehyde, 8-hydroxy-, oxime 118 ■ i 1 • 1 1 i ■7 1 ri ■ । >■ । । ■ । । । । । 25.20 25.40 25.60 25.80 5000 m/z 184.05 10.65% 143 64 158 170 89 116 130 . PP*Pmm=-I1 mPP L rp-r m/z—> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19873:4H-Pyrido[1,2-alpyrimidin-4-one, 3-ethyl-6-methyl- ■ i 1 ■ 1 ‘ i ■7 ■ 1 i 1 ■ 1 ■ i ■ ■ 1 ■ i ■ 145 1118 25.20 25.40 25.60 25.80 173 m/z 158.05 8.96% 5000 92

119 132 159 ।" <11 < • ■ 11111 > ।'1 ■111 m 1 ,,,,, ,iHp ...... Ii,.... ■ i ' ' ' ' I *Ti r । । । . mfe-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 25.20 25.40 25.60 25.80

12538.D GCMS0531.M Tue Jun 04 11:52:07 2002 Page 2

NYC-WTC_000014668

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NYC-WTC_000014670

Laboratory report documenting GCMS analysis of sample AE12539 conducted on June 7, 2002, including surrogate recovery data.

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