GCMS analytical report for sample AE10607 showing unknown compounds and surrogate recovery data from May 15, 2002.
NYC-WTC_000045423–000045433Folder label: “GCMS X 5/3/02 A 5/8/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\HPCHEM\l\DATA\MAY0802\10607.D Vial: 6 Acq On 8 May 2002 3:27 pm Operator: Sample GC/MS SCAN 5/3 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0507.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Phenanthrene-diO Concentration Rank 3
R.T. EstConc Area Relative to ISTD R.T.
25.72 0.44 ug/1 36303 Phenanthrene-dl0 25.57
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Phenanthrene-dl0• 2 188 C14D10 001517-22-2 72 2 Anthracene-d10- 188 C14D10 001719-06-8 40 3 4H-Pyrido [1,2-a]pyrimidin-4-one, 3- 188 C11H12N2O 057773-19-0 40 4-(4-Tolyl)-3-methyl-pyrazol-5-one188C11H12N20 035496-19-6 38 Abundance Scan 2256 (25.716 min): 10607.D (-) m/z 188.15 100.00% 188
5000
80 94 J r ■ I T ' | 1 > 1 ' | 1 ■ ■ ■ |
42 52 66 156 25.40 25.60 25.80 26.00 ....... iL nnnd l I I I I I I I I 11111111 " 11 — m/z 189.15 18.15% m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19958: Phenanthrene-d10 188
/ 5000 i i । i i I I | i I|| I | 1' i 1' I I T’ I I 'j
25.40 25.60 25.80 26 00 m/ z 80.10 14.99% 80 94 160 66 m/z-> 40 50 60 70 80 — i' ■ ■11
90 100 110 120 130 140 150 160 170 180 190 TPPTP ...... IJ... Abundance #19957: Anthracene-d10- 188
25.40 25.60 25.80 26.00 5000 m/ z 94.10 12.32%
80 94 160 66 ■ | ■ 11 I ■ ■ । r ■1 ■ 11 ' j '1 । > i ■ ■ ■ ■ । ■ I " 1' I 11 " 11 1 . r ' I' 11 ' I' m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170_180_190 Abundance #19873: 4H-Pyrido[1,2-a]pyrimidin-4-one, 3-ethyl-6-methyl- ’5 1U ।/_ ........ 'r । । । । ....................... r । । i i i -i-| ■ । i r 1 ।
145 188 25.40 25.60 25.80 26.00 173 m/z 184.15 9.49%
5000 92
65 159 119 132 ______ / ___________________ TT 1 I ‘ ' 1 1 I - UI 11111 I''' 'I 11 '1 11 11 11 I । | । i । i | I r I I | I I I I [ l I I J
m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 25.40 25.60 25.80 26.00
10607.D GCMS0507.M Thu May 09 14:42:17 2002 Page 3
NYC-WTC_000045432
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Ranked by indexed similarity. Reasons describe shared subjects and filing context; check the source records.
NYC-WTC_000044836
Laboratory report showing gas chromatography-mass spectrometry results for unidentified organic compounds in sample AE10165 on May 10, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000044804
Laboratory report documenting GCMS analysis of sample AE10159 conducted on May 10, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000044815
Laboratory report documenting GCMS analysis of sample AE10161 conducted on May 10, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000044338
Laboratory comment noting low recovery in initial GCMS scan of sample AE08264, resulting in re-extraction.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000045247
Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE10434 conducted on May 20, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043291
GCMS results for sample AE09521 showing surrogate recovery and unknown compounds dated May 6, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000045353
GCMS analytical report for sample AE10519 focusing on unknown compounds from May 21, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000045386
GCMS analytical report for sample AE10522 showing unknown compounds and surrogate recovery data from May 22, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000044349
Laboratory report documenting GCMS analysis of sample AE09565 conducted on May 6, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043472
Laboratory report of GCMS analysis for sample AE07107 including surrogate recovery data from April 29, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023316
Laboratory report showing GC/MS analysis results for sample AE09578 including surrogate recovery data on May 16, 2002.
1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000014680
Laboratory report documenting GCMS analysis of sample AE12570 conducted on June 7, 2002, including surrogate recovery data.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000045396
Department of Environmental Protection GCMS analysis record for the World Trade Center site dated May 3-8 2002.
Filed in the same folder
NYC-WTC_000045397
Single fragmented page from a Department of Environmental Protection record dated May 3, 2002 with illegible content.
Filed in the same folder
NYC-WTC_000045400
GCMS blank analysis report for sample AE09447 listing compounds below detection limits from May 8, 2002.
Filed in the same folder
NYC-WTC_000045411
GCMS calibration report for sample AE09447 showing recovery percentages for various compounds from May 8, 2002.
Filed in the same folder
NYC-WTC_000045415
GCMS reference standard report for sample AE09447 showing quantified compound levels from May 8, 2002.
Filed in the same folder