GCMS analysis results for sample AE07484, May 2002

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Laboratory report documenting GCMS analysis of sample AE07484 conducted on May 6, 2002, including surrogate recovery data.

NYC-WTC_000044268–000044278

Folder label: “GCMS X 4/23/02 A 4/26/02”

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NYC 9/11 Public Portal Document

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Data File : C:\HPCHEM\l\DATA\APR2502\7484.D Vial: 7 Acq On : 26 Apr 2002 11:15 pm Operator: Sample : gc/ms scan 4/23 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Phenanthrene-diO Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T. 25.72 0.23 ug/1 36681 Phenanthrene-dl0 25.58 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthyene-410%7 188 C14D10 001517-22-2 53 2 Anthracene-d10- 188 C14D10 001719-06-8 50 3 -(4-Tolyl) -3-methyl-pyrazol-5-one 188 C11H12N2O 035496-19-6 38 4 4H-Pyyido[1,2-a] pyrimidin-4-one , 3- 188 C11H12N2O 057773-19-0 9 Abundance Scan 2252 (25.722 min): 7484. D (-) m/z 188.10 100.00% 188

5000

। । । । । । > । 1 । r । । i i । । । । । । 1

44 66 80 94 160 1 I r-] I ri I | । I i r i i i i । 4 25.40 25.60 25.80 26.00 11 r 11 ■ i111' r 1' ‘ i ‘ I ‘111111111 | IIr m/ Z 94.00 12.77% m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19958: Phenanthrene-d10 188

/ 5000 1 l ~ I ' 1 1 1 I 1 1 1 ' I 25.40 25.60 25.80 26.00 m/z 184.00 12.01% 80 94 160 66 . I i I I | i i i i । । i ! । । |1111 L i i t r — I ' ' ■ ' I 1 1 I ' 1 1 1 I m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19957: Anthracene-d10- 188 i । _|_ i— r I । । 1 । “ । । r ■i । । । । i ITT

25.40 25.60 25.80 26.00 5000 m/z 160.05 10.63%

80 94 160 66 ■ |■111■11।11111111111 ■ ■111 r ■ i ■ > ■ ■ i ■ > ■ > । ■ I ■ । T-p-r miz-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19863: -(4-Tolyl)-3-methyl-pyrazol-5-one ■ ■ ( ■ ■ ■ ■ | t- । i-, ! , . . , । । । 188 25.40 25.60 25.80 26.00 91 m/z 189.10 9.38% 105 5000 119 65 78 i । । । । । । । । । । । । । । । । ] r guni । । I । । । । । ।I I i । । । । । । । । । i । r i ) i । 146 tI I' I I I I I I I I I I I 1 I I I I I I I I ...... 1............... । । । । ।' । । । iiii pn । । । । i n—[—|" m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 25.40 25.60 25.80 26.00

7484.D GCMS0412.M Thu May 02 05:34:21 2002 Page 3

NYC-WTC_000044277

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