GCMS calibration table for TCLP method, March 2002

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Instrument output displaying calibration data and surrogate recovery results for sample AE03380.

NYC-WTC_000011477–000011484

Folder label: “GCMS X 2/14/02 A 3/2/02 - 3/20/02”

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NYC 9/11 Public Portal Document

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Data File C: \HPCHEM\ 1 \DATA\MARO 102\3380.D Vial: 44 Acq On 3 Mar 2002 6:37 am Operator: Sample gc/ms scan 2/4 fb Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Phenanthrene-diO Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

25.86 0.32 ug/1 96320 Phenanthrene-dl0 25.73

Hit# of 5 'entative ID MW MolForm CAS# Qual

1 Phenanthrene -d10 c 188 C14D10 001517-22-2 72 2 Anthracene-d10- y / 188 C14D10 001719-06-8 50 3 4-Methyl/2-(3-fluorophenyl)pyrimidi 188 C11H9FN2 076128-66-0 50 4 -(4-Tolyl)-3-methyl-pyrazol-5-one 188 C11H12N2O 035496-19-6 40 Abundance T Scan 2267 (25.857 min): 3380.0 (-) m/z 18 .10 100.00% IBS

5000

80 94 66 146 160 25.60 25.80 26.00 26.20 42 mtn118 .......... I if 1 1 ' 1 1 reri | 1 I M 132 54 | I 1 I I | I 1 1 1 | I I I I" , . , | . nillan n m/z 79.95 15.88% m/z-> 40 50 60 70 80 90.100 110 120 130 140 150 160 170 180 190 Abundance #19958: Phenanthrene-d10 188

5000 25.60 25.80 26.00 26.20 m/z 189.10 13.93% 66 80 94 160 mLLTTTTRTIPTT I " ‘11 m/z-> 40 50 80 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance het 1 188

25.60 25.80 26*oo '26'20 5000 m/z 184.00 12.87%

66 80 94 160 “ । ■1 ■ ■ 1■ “ ■।1 ■ 1 ■ ■ ■ • । • • ■ ■ । ■ ■ ■ ■ । ■i•■ “ ।■ ■ ■ ■ । ■ ■ ■ ■ । ।। < • •■। ।■■■ ■ । । ............................................... m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190__ Abundance #19859:4-Methyl-2-(3-fluorophenyl)pyrimldine 188 25.60 25.80 26.00 26.20 m/z 94.00 11.09% 5000 121

173 67I 75, 94Il 146 161 | 11'' ‘ ■ i ‘ ' i ■ mrrgini 1* '' i' “ ' i ‘'1 ■ i ■1'11 ■1 •' i ■''' i " I"1‘I . . , .1 . t l . . । . . . . । . m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 25.60 25.80 26.00 26.20

3380.D GCMS0208.M Mon Mar 25 12:20:06 2002 Page 2

NYC-WTC_000011483

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