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GCMS blank analysis results, DEP Labs, Feb 2002

Machine-extracted title · confidence 100%

GCMS blank sample results for target compounds showing non-detectable levels on February 22, 2002.

NYC-WTC_000009807–000009815

Folder label: “GCMS X 1/22/02 A 2/22/02

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Scanned page image, NYC-WTC_000009814
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\FEB2102\LB.D Vial: 3 Acq On : 21 Feb 2002 4:03 pm Operator: Sample : gc/ms scan 1/22 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Phenanthrene-diO Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

25.88 0.23 ug/1 22390 Phenanthrene-dl0 25.73

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Phenanthrene -d10 C 188 C14D10 001517-22-2 78 2 Anthracene-d10- X 188 C14D10 001719-06-8 64 3 4-Methyl-2-(4-fluorophenyl)pyrimidi 188 C11H9FN2 076128-67-1 53 4 4-Methyl 2-(3-fluorophenyl)pyrimidi 188 C11H9FN2 076128-66-0 53 Abundance Scan 2270 (25.878 min): LB.D (-) m/z 18 .10 100. 00% 188 i

5000 — 40 80 94 160 — 25.60 25.80 26.00 26.20 __ 6611]... 11..................... m/z->..... 30... 40... 50.... 60 70 80 90 100 110 120 130 140 150 160 170 180 190 m/Z—39:95—25,385 Abundance #19958: Phenanthrene-dib 188

5000 25.60 25.80 26.00 26.20 m/z 160.05 17.83% 80 94 160 ------- m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance 188

25.60 25.80 26.00 26.20 5000 m/z 157.95 15.10%

. 66 80 94 160

m/z-> 30 40. 50 60. 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19860:4-MethyT-2-(4-fluoropfienyi)pyrimidine /nnnmBnBB/non 188 25.60 25.80 26.00 26.20 121 m/z 93.95 13.85% 5000 173 67 94 57 [ 75 |, 102 146 1 .......... ................................ 11111’11211011’211091t22713* ’1 ■' i “ “ i ■ • r' i' “ ‘ i' “ ‘ i' TTTur 14s m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 25.60 25.80 26.00 26.20

LB. D GCMS0208.M Fri Feb 22 09:43:55 2002 Page 2

NYC-WTC_000009814

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NYC-WTC_000009814Source: NYC Law Department, mirrored locally

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