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GCMS analysis results for sample AE02598, Mar 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of unknown compounds in sample AE02598 conducted on March 7, 2002.

NYC-WTC_000005291–000005301

Folder label: “GCMS X 2/5/02 A 3/1/02

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Scanned page image, NYC-WTC_000005299
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NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\HPCHEM\l\DATA\MAR0102\2598 .D Vial: 8 Acq On 1 Mar 2002 3:14 pm Operator: Sample gc/ms scan 2/5 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 4-Methyl-2-(3-fluorophenyl)pyr Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

25.85 0.25 ug/1 28390 Phenanthrene-dl0 25.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 4-Methyl-2-(3-fluorop yl)pyrimidi 188 C11H9FN2 076128-66-0 45 2 4-Methyl-2-(4 fluorop yl)pyrimidi 188 C11H9FN2 076128-67-1 45 3 Anthracene -d10- J y 188 C14D10 001719-06-8 43 4 Phenanthrene -diO 188 C14D10 001517-22-2 28 Abundance / Scan 2267 (25.854 min): 2598.D (-) j m/ z 188.1 0 1 00.0 o % 188

5000 ............ ... ..................................... 94 44 66 80 160 । t____ 25.60 25.80 26.00 26.20 J PmeummBmTtnp T-TTTT I r — m/z 184.05 14.57% m/z-? 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190i i A Abundance #19859: 4-Methyi-2-(3-fluorophenyl)pyrimidine 188

- 5000 121 25.60 25.80 26.00 26.20 67 173 m/z 93.90 13.48% 75 94 146 161 i 1I1"‘50111010111721101000-n‘1Tf091010UIUIIT m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance

5000 121 188 A25.60 25.80 26.00 26.20 m/ z 189.00 7.78% 173 67 94 57 75 102 146 m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 . ... ....... Abundance #19957: Anthracene-cHO- 188 25.60 25.80 26.00 26.20 m/ z 160.05 7.63% 5000

66 80 94 160 0*** ----- - m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 25.60 25.80 26.00 26.20

2598.D GCMS0208.M Mon Mar 04 11:42:35 2002 Page 2

NYC-WTC_000005299

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NYC-WTC_000005299Source: NYC Law Department, mirrored locally

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