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GCMS analysis results for sample AE02598, Mar 2002

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Laboratory report documenting GCMS analysis of unknown compounds in sample AE02598 conducted on March 7, 2002.

NYC-WTC_000005291–000005301

Folder label: “GCMS X 2/5/02 A 3/1/02

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\HPCHEM\1\DATA\MARO102 \2598.D Vial: 8 Acq On 1 Mar 2002 3:14 pm Operator: Sample gc/ms scan 2/5 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Decanedioic acid, bis(2-ethylh Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

36.25 8.52 ug/1 596543 Perylene-dl2 38.05

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Decanedioic acid, bis(2-ethylhexyl) 426 C26H50O4 000122-62-3(91 2 [1,11-Biphenyl]-4-ol, 3-amino- 185 C12H11NO 001134-36-7 35 3 Pyridine, 4-[4-methoxyphenyl]- 185 C12H11NO 000000-00-0 17 4 Propanedioic acid, hexyl-, diethyl 244 C13H2404 005398-10-7 14 Abundance Scan 3400 (36.255 min): 2598.D () m/z 185.10 100.00% 185

57 5000 43 70 112 - 83 98 36.00 36.20 36.40 36.60

m/z--> ''40A'A60, A,80'l 100 120125 140 143 166 203 .1 t. J l„ 255268231 297 315 160 180 200 220 240 260 280 1. ! m/z 57.0^0 52.95 % 300 320 i Abundance #55661: Decanedioic acid, bis(2-ethylhexyl) ester 185

57 ) 5000 ■ ' | ' T IIIT74IIII 71 112 36.00 36.20 36.40 36.60 ; m/z 70.1,0 38.01%

mZ— 40 —P60 M 84 98

80 125 143 166 203 298 316 ' i 1 1 ■ ■ i ■ ■ ' ‘ I ' 1 1 1 i 1 ' 1 1 i ' ■ 1 ■ i 1 1 1 1 I ' 1 ' 1 1 1 1 1 1 I ' 1 1 'I ' 1 ' 1 1 1 100 120 140 160 180 200 220 240 260 280 300 320 Abundance 185 / 36.00 36.20 36.40 36.60 5000 | m/z 71.10 36.4 8% 139 156 : ■ 113 । m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #19196: Pyridine, 4-[4-methoxyphenyl]- 11 I ' T 1 * f 1 ' 1 ' I ‘ 1 1 1 I 1 ‘ ‘ ; 185 36.00 36.20 36.40 36.60 ! m/ z 55.00 32.30%! 5000- 142 115 170 83 89 —

m/z-> .... 4.78,47...4,1 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 36.00 36.20 36.40 36.60

2598.D GCMS0208.M Mon Mar 04 11:42:40 2002 Page 3

NYC-WTC_000005300

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NYC-WTC_000005300Source: NYC Law Department, mirrored locally

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