GCMS analysis results for sample AE02602, Mar 2002

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Laboratory report documenting GCMS analysis of sample AE02602 conducted on March 7, 2002, including surrogate recovery data.

NYC-WTC_000005322–000005332

Folder label: “GCMS X 2/5/02 A 3/1/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\MAR0102\2602.D Vial: 12 Acq On 1 Mar 2002 7:11 pm Operator: Sample gc/ms scan 2/5 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 4-Methyl-2-(3-fluorophenyl)pyr Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

25.85 0.23 ug/1 24816 Phenanthrene-dl0 25.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 4-Methyl-2 (3-fluorophenyl)pyrimidi 188 C11H9FN2 076128-66-0 45 2 4-Methyl -2/- (4-fluorophenyl) pyrimidi 188 C11H9FN2 076128-67-1 45 3 Anthracene-dl0 - 188 C14D10 001719-06-8 38 4 Phenanthrene-diO 188 C14D10 001517-22-2 9 Abundance Scan 2267 (25.852 min): 2602.D (-) '88 ! m/z 188.10 100.00%

5000 — 49 66 80 9,“ 160 25.60 25.80 26.00 26.20 - 1111 ।11 111 111 । 1 11 ! ।! ! !! । —T I rt m/z 18 4.05 13.88% । ■ ■'' ।' ■'' । I m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19859: 4-Methyl-2-(3-fiuorophenyl)pyrimidine 188

— 5000 121 25.60 25.80 26.00 26.20 67 173 m/z 66.05 13.53% 94 ............ 175 I ■ ■ ■ 1 । ■ > ‘ ' । 1 1 1 1 I 1 1 ' 1 1 ' — 146 161 । ■1 ■11' ■ ■' । ■1 ■ । ■ ■ ■' ।' i ।'' ■' । ■ It’ m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance 188

121 25.60 25.80 26.00 26.20 5000- m/z 94.00 11.43% 173 67 94 57 75 102 146 I ''' ‘ i' '' ■ i'''11''' ' i' ‘iT i' ■ ■' i ■ • ■' i | ‘ ‘ | ‘ ‘ | ‘‘ | ‘ ‘ | ' 1 *I . i r

m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19957: Anthracene-d10- ,................. 188 25.60 25.80 26.00 26.20 m/z 187.20 9.67% 5000

— 80। 94 160 ob - — l ■ ■ ■ ' I ' 1 ' ■ I 1 ' 1 ' i ' ' 1 ' I ' ' 1 T-p-T m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 25.60 25.80 26.00 26.20

2602.D GCMS0208.M Mon Mar 04 11:46:24 2002 Page 2

NYC-WTC_000005330

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NYC-WTC_000005330Source: NYC Law Department, mirrored locally

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