GCMS calibration table with surrogate recovery data, Feb 24, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report 5 * Data File : C:\HPCHEM\1\DATA\FEB2102\942.D Vial: 64 Acq On : 24 Feb 2002 7:05 am Operator: Sample : gc/ms scan 2/21 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 Anthracene-dlO- Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

25.88 0.22 ug/1 17826 Phenanthrene-dl0 25.73

Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Anthracene-d10- 188 C14D10 001719-06-8 90 2 Phenanthrene7dl0 188 C14D10 001517-22-2 80 3 4-Methyl-2 fluorophenyl)pyrimidi 188 C11H9FN2 076128-67-1 40 4 4-Methyl-2 fluorophenyl)pyrimidi 188 C11H9FN2: 076128-66-0 40 Abundance 1 Scan 2269 (25.876 min): 942.D 0 T 7 1 T m/z..188.10.... 100.00% 188

5000

94 160 66 80 25.60 25.80 26.00 26.20 -- • • i • ■»■ i -I 1 * ’ ’ * 1 1 ’ * ‘ I' ‘ ‘ I TTT m/z 160.05 15.96 m/z-50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19957: Anthracene-d10- 188

... y i । । । । । । । > । 5000 25.60 25.80 26.00 26.20 80 94 m/z 184.10 15.55% 160 66 ' I ri pthji miz-2.... 50__ 60 70 L I ‘ ‘ ‘ ’ I *' ' ‘ I ‘ 8090 1Q0 110 120 130 140 150 160 170 180 190 ' I ‘ ‘ ’ I sI. T l Abundance 188

25.60 25.80 26.00 26.20 5000 m/z 93.90 15.50

66 80 94 160 ‘ i ■ ■ ‘ ■ i1 ‘ ■ i ‘ ■ i ■ ■ ■ ■ । •1 i" • ■ ।। ■ ■ • ■ । । ■ ■ ■ ■ । ■ i1 ■'111111111 ■' ■ i1' miz-> 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19860:4-Methyl-2-(4-fluorophenyl)pyrimidine 188 25.60 25.80 26.00 26.20 121 m/z 158.05 11.93% 5000 173 67 94 57 1’| 1’75 |, 102 146 ------- ■ i' ■ ‘ ■ i ‘ 1 ’111211117112 ———" —— T’r ■ ■ i •''11 ■ ■1 ■ i ■ ‘ • i • ■ ■ ■ i • m/z-> 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 25.60 25.80 26.00 26.20

942.D GCMS0208.M Fri Mar 01 09:13:30 2002 Page 4

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