GCMS analysis results, Sample AE08432, April 18, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\APR1202\8432.D Vial: 21 Acq On : 16 Apr 2002 3:41 am Operator: Sample : gc/ms scan 4/10 fb Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 2 Anthracene-dlO- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

25.75 0.29 ug/1 56942 Phenanthrene-dl0 25.61

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-d104 188 C14D10 001719-06-8 91 2 4-Methyl2- (3-f luowphenyl) pyrimidi 188 C11H9FN2 076128-66-0 50 3 4-Methy.-2- (4-fluorophenyl)pyrimidi 188 C11H9FN2 076128-67-1 50 4 Naphthalene, 2,6-dimethoxy-________ 188 C12H1202 005486-55-5 40 Abundance Scan 2255 (25.750 min): 8432. D (-) m/z 188.10 100.00% 188

5000

94 ...bam) 40 49 66 80 25.40 25.60 25.80 26.00 । > । । | । i । i । rri i| i i I । । । । । I | । । । i I i . .... .......... ।... m/ z 94.00 16.32% mlz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19957: Anthracene-d10- 188

5000 m 25.40 25.60 25.80 26.00 m/z 189.10 12.61% 66 80 9|4 IfO mPTTTTTTTTmTTTT m/z—> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19859:4-Methyl-2-(3-fluorophenyl)pyrimidine 188 ............. .......... .......................... I I I I I I I I I I I I I I I II I I’I 1

25.40 25.60 25.80 26.00 5000 121 m/z 184.00 9.49%

173 67 75 94 175... 1......... i........ 146 161 I......। ' " i11 " i1''11'1111 " 111" " r i i i i । i > i i । i i r i । ii i i । iii i|ii । । । । । I m/z—> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19860: 4-Methyl:2-(4-fluorophenyl)pyrimidine I i | i i । r । i I i T | I i i r | I I i i | i 188 25.40 25.60 25.80 26.00 m/z 160.05 9.47% 121 5000

173 67 94 . — ............ 57 J| 75........ I CL7u 102........... J1 i i ITI 146 । < >'[ । ri। । । । । । <i| i i i ] i । । । । । । |i । । । ।■ । ■ i ■ i ■ ■ ■ ■ 11 । । ■ IIur ITT r । rr T." m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 25.40 25.60 25.80 26.00

8432.D GCMS0412.M Wed Apr 17 09:47:30 2002 Page 2

NYC-WTC_000048538