GCMS Method 508 analysis worksheet, May 2002

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Library Search Compound Report .> Data File : C:\HPCHEM\1\DATA\MAY29O2\LBA.D Vial: 16 Acq On : 30 May 2002 2:04 am Operator: Morgan Sample : gc/ms scan 5/23 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0528.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Anthracene-dlO- Concentration Rank 3

R.T. EstConc Area Relative to TSTD R.T.

25.57 0.42 ug/1 45188 Phenanthrene-dl0 25.42 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Anthracene -d10- 6 188 C14D10 001719-06-8 78 2 Phenanthrene-dl0 z 188 C14D10 001517-22-2 78 3 4-Methyl-2- (3-fluorophenyl)pyrimidi 188 C11H9FN2 076128-66-0 42 4 4-Methyl/2-(4-fluorophenyl)pyrimidi 188 C11H9FN2: 076128-67-1 42 Abundance Scan 2236 (25.571 min): LBA.D (-) m/z 188.10 100.00% 1118

5000 ....... 1 ----- • I ‘ ‘ 1 ‘ I ' 80 94 25.20 25.40 25.60 25.80 26.00 156 miz-> 42 TVPTr 66 H ■ ■ i ‘ " i ■ ■ “ i ‘ ■ i"' ■ i “ “ i ■ ■ । ''I ‘ " i ■ ■ ■111 1’1 m/z 94.05 13.85% 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19957: Anthracene-d10- 118

5000 25.20 25.40 25.60 25.80 26.00 m/z 189.10 12.49% 94 66 80 -pmmmmP “ i" “ i ■ •' ■ i" ■ ■ i ■" ■ i • ■ “ i ■ miz—> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19958: Phenanthrene-d10 118

25'20 25.40 25.60 25.80 26.00 5000 m/z .95 10.89%

80 94 160 66 mz-> ’ 1’11111 i111 > i - 4 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 . .... Ill... Abundance #19859: 4-Methyl-2-(3-fluorophenyl)pyrimkfine 1118 2620 25.40 25.60 25.80 26.00 m/z 184.10 9.64% 5000 121

173

miz—> ■ " i “ “ r ■ “ i ‘ 77 146 161 | | TTTTTTT’—’::1111211230-221113 1 | 1 1 I 1 | 1 1 1 1 | ■ > 1 1 । rt r > । 1 1 1 1__ 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 113 25.20 25.40 25.60 25.80 26.00

LBA.D GCMS0528.M Thu May 30 10:39:52 2002 Page 3

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