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GCMS blank analysis for sample AE04038, Mar 27 2002

Machine-extracted title · confidence 100%

Quality control blank analysis results for GC/MS testing of sample AE04038 conducted on March 27, 2002.

NYC-WTC_000011698–000011706

Folder label: “GCMS X 2/25/02 A 3/23/02

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Scanned page image, NYC-WTC_000011705
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\MAR2 202\LBA.D Vial: 16 Acq On : 23 Mar 2002 10:50 am Operator: Sample : gc/ms scan 2/25 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Anthracene-dlO- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

25.80 0.23 ug/1 35361 Phenant hrene-dlO 25.66

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-d10- 188 C14D10 001719-06-8 47 2 PentacVclo[8.4.0.0(3,7).0(4,14).0(6 188 C14H20 000000-00-0 38 3 Phenanthrene-d10 188 C14D10 001517-22-2 37 4 Cyclohexanone , phenylhydrazone 188 C12H16N2 000946-82-7 36 Abundance Scan 2260 (25.797 min): LBA.D (-) 1 m/z 188.10 100.00% 188

5000

66 80 94 25.40 25.60 25.80 26.00 26.20 40 mmp 4l — m 132 160 , m/z~>30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 l ’ ! m/z 189.00 19.57% Abundance #19957: Anthracene-d1 0- 188

5000 25.40 25.60 25.80 26.00 26.20 m/z 94.00 14.81% 66 80 94 160 TTPWPmemmmmmmpugp m/z—> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance '14,0(6 11 tel 0 orano 188

25.40 25.60 25.80 26.00 26.20 5000 m/z 80.00 11.46% 79 92 117 106 131 145 159 173 T ' i ■1 ■' i ■ ■ " i " TTuan] m/z30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19958: Phenanthrene-d10 188 25.40 25.60 25.80 26.00 '26'20 m/z 78.05 9.23% 5000

80 94 160 - 66 ■ ■ i ■" ■ i “1 ■ i “ । • i" m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 25.40 25.60 25.80 26.00 26.20

LBA.D GCMS0308.M Wed Mar 27 10:12:07 2002 Page 2

NYC-WTC_000011705

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NYC-WTC_000011705Source: NYC Law Department, mirrored locally

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