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GCMS analysis results for sample AE04128, April 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE04128 conducted on April 1, 2002, by analyst DLV.

NYC-WTC_000011767–000011778

Folder label: “GCMS X 2/25/02 A 3/23/02

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Scanned page image, NYC-WTC_000011777
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\MAR2202\4128.D Vial: 24 Acq On : 23 Mar 2002 6:44 pm Operator: Sample : gc/ms scan 2/25 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Anthracene-dlO- Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

25.79 0.22 ug/1 33197 Phenanthrene-dl0 25.66 / Hit# of Tentativ 5 ID MW MolForm CAS# Qual 1 Anthracene -a12- 7 ------------------------ -- 188 C14D10 001719-06-8 (87 2 Phenanthrene/dlO 188 C14D10 001517-22-2 83 3 Phosphonic acid, (3-methyl-3-penten 188 C8H13O3P* 022152-34-7 40 4 Pentacyclo DB . 4.0.0(3,7) .0(4,14) .0(6 188 C14H20 _____ 000000-00-0 33 Abundance 7 Scan 2260 (25.795 min): 4128.D (-) 1m/ z 188. 10 100.0 6% 188

5000

40 66 80| 94 160 25.40 25.60 25.80 26.00 26.20 " 111111111111"11"1111111111 —WmPmmmmm 1’’ m/z 187.20 25.78% m/z-> 30.. 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19957: Anthracene-d10- 188

5000 25.40 25.60 25.80 26.00 26.20 m/z 189.10 21.92% 66 80 94 TmImmmmmpmmg 160 i “ “ i" TTT m/z-> 30 40 50 60. 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #1 9G53: Phenanipene-d 10 188

25.40 25.60 25.80 26.00 26.20 5000 m/z 7 .95 14.11%

66 80 94 160 TmmmmmmmmmmmmTTT m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19736: Phosphonic acid, (3-methyl-3-penten-1-ynyl)-. dimet 188 25.40 25.60 25.80 26.00 26.20 m/z 184.05 11.40% 5000 77 62 93 + m 35 47 109 155 111101111 ■ • 1 ■: ■ T TTTTT ।■■■•। 1’1 m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 25.40 25.60 25.80 26.00 26.20

4128.D GCMS0308.M Wed Mar 27 10:04:20 2002 Page 3

NYC-WTC_000011777

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NYC-WTC_000011777Source: NYC Law Department, mirrored locally

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