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GCMS analysis results, sample AE04801, Apr 2002

Machine-extracted title · confidence 90%

Gas chromatography-mass spectrometry analysis of environmental sample AE04801 conducted April 4, 2002, detecting unknown compounds and surrogates.

NYC-WTC_000058325–000058338

Folder label: “GCMS X 3/4/02 A 3/23/02

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Scanned page image, NYC-WTC_000058333
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\MAR2802\4801.D Vial: 13 Acq On : 28 Mar 2002 8:27 pm Operator: Sample : gc/ms scan 3/4 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Anthracene-dlO- Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

25.77 0.23 ug/1 31354 Phenanthrene-dl0 25.63

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Anthracei^-dlO- A 188 C14D10 001719-06-8 72 2 PhenantlUene-dlO \ 188 C14D10 001517-22-2 56 3 -(4-Tol/l)-3-methyl-pyrazol-5-one 188 C11H12N2O 035496-19-6 40 4 Benzalipehyde, 2,6-dif luoro-4-hydrox 188 C8H6F2O3 000000-00-0 28 Abundance ” ” ” ... Scan 2257"(25.”768"minpOOtD {-)” ” ..... . m/z 188.10“" 100.”00% 1«8

5000

94 ....... y \..................... 66 80 156 25.40 25.60 25.80 26.00 4S m/z 94.00 19.01% m/z-> 40.. 50... 60 70.... 80.... 90... 100 J10 J 20 130 140 150 160.. 170 J8p_190 Abundance #19957: Anthracene-diO- 188 i 5000- ■p" 2540 25.60 25.80 26.00 fiR • SO 94 m/z 189.10 16.77% 160 I DO ! Xt Ui iD/Zch.___ 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 'Xbundance #19956. Phaiianthrene-ciiO I 188 I ii ' 25.40 25.60 25.80 26.00 5000 m/z 184.10 14.93%

80 94 160 66 .......... I ' ' ' ' I p ‘ I m/z-> 40 50 60 70 80 90 100 110 120 130140 150 160 170 180 190 Abundance #19863: -(4-Tolyl)-3-methyl-pyrazol-5-one i like 25.40 25.60 25.80 26.00 i 91 m/z 80.00 12.92% 105 5000 119 146 'm/z-: 40 50 60 70 80 90100 110 120 130 140 150 160 170 180 190 25.40 25.60 25.80 26.00

4801.D GCMS0308.M Mon Apr 01 10:15:20 2002 Page 2

NYC-WTC_000058333

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NYC-WTC_000058333Source: NYC Law Department, mirrored locally

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