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Laboratory method sheet for liquid-liquid extraction parameters

Machine-extracted title · confidence 90%

Technical record detailing laboratory method parameters including drip rates and reagent volumes for sample processing.

NYC-WTC_000059589–000059598

Folder label: “GCMS X 3/12/02 A 4/4/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\APRO3 02\LBA.D Vial: 15 Acq On 4 Apr 2002 8:27 am Operator: Sample gc/ms scan 3/12 Inst : GC/MS 209 Mise : Multiplr: 2.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0408.M (RTE Integrator) , Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Anthracene-dlO- Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 25.77 0.44 ug/1 39304 Phenanthrene-dl 0 25.63 Hit# of •5 Tentative ID MW MolForm CAS# Qual 1 Anthracene-diO- 0^^ 188 C14D10 001719-06-8 64 2 Phenanthrene/-dl 188 C14D10 001517-22-2 38 3 l,4-Naphtha]/enedione, 2-hydroxy-3-m 188 C11H8O3 • 000483-55-6 9 4 Benzene, l-/l-cyclohexen-l-yl)-4-me 188 C13H16O 020758-60-5 9 Abundance / Scan 2258 (25.774 mill): LBA.D (-) m/z 188.10 100.00% 1$8

5000 94 52 66 80 160 25.40 25.60 25.80 26.00 26.20 I' '' ' I''' ‘ I m/z 94.00 22.66% Ti/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19957: Anthracene-dlO- 188

553 25 40 25.60 25.80 26.00 26.20 m/z 189.10 20.49% 80 94 160

TiZz-> 40 ....... ..... I. 90 100 110 120 130 140 150 160 170 180.. 190 50 60 70 80 Abundance #19958: Phenanthrene-dlO 188

2540 25.60 25.80 26.00 26.20 5000 m/z 184.10 17.82%

80 94 160 66 Xr ............... T.-iq.,-. 7l/z-> 40 Abundance 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 #69174:1,4-Naphthalenedione, 2-hydroxy-3-methyl- 1(18 w 25.40 25.60 25.80 26.00 26.20 m/z 65.95 8.36%

5000

IOS 131 ,go 50 ■n" nri/z-> 40 50 60 90 100 110 120 130 140 150 160 170 180 190 25.40 25.60 25.80 26.00 26.20

LBA.D GCMS0408.M Tue Apr 16 08:15:36 2002 Page 3

NYC-WTC_000059597

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NYC-WTC_000059597Source: NYC Law Department, mirrored locally

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