GCMS sample analysis summary, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\bATA\MAR3002\4941.D Vial: 8 Acq On : 29 Mar 2002 9:53 pm Operator: Sample : gc/ms scan 3/6 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Anthracene-dlO- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

25.77 0.22 ug/1 36465 Phenanthrene-dl0 25.63

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Anthracene-diZ- \ 188 C14D10 001719-06-8 50 2 Phenanthren^dlO \ 188 C14D10 001517-22-2 50 3 Pentacyclo/8.4.0.0(3,7) .0(4,14) .0(6 188 C14H20 000000-00-0 45 4 Naphthale/e, 2,6-dimethoxy- _________ 188 C12H12O2 005486-55-5 40 Abundance Scan 2257 (25.769 min): 4941.D (-) 1“m/z 188.10 100.00^ 1$8

5000

160 25.40 25.60 2^80 26.00 ' ...,I . Ph . , . m/z 189.10 16.86% 'm/z-> 30 40 50 60 70 80__90 100 110_120 130 140 150 160 170 180 190 Abundance #1'9957: Anlhrace'ne-dlO-.. ... .... ...... . 188 i

5000 25.40 25.60 25.80 26.00

cc 80 94 m/z 92.00 15.54% 160 I ,1 Trr| r. 1 ■ । > > > ■ । I > > > ) — m/z->30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19958 Pnsnanthrene-dl6 i 188

_.25.4O_ 25^60 _25J0 26.00 5000

'm/z-> Abundance 30 40 50 60 66

70 80 94 T' ‘' I 160

90 100 110 120 130 140 150 160 170 180 190 #19959: Pentacyclo[8.4.0,0(3.7).0(4.14).0(6,11)]tetradecane 1$8 I. p -.-.. I III I I "7 .. 25.40 25.60 25.80 26.00 m/ Z 9.95% 5000

I I I 106 131 145 159 173 ! ,., ■ , l{ I , I II, '| J , I, 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 25.40 25.60 25.80 26.00

4941.D GCMS0308.M Tue Apr 02 11:05:35 2002 Page 2

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