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GCMS sample analysis summary, April 2002

Machine-extracted title · confidence 100%

Summary page for GCMS analysis of sample AE04941 conducted on April 5, 2002.

NYC-WTC_000058649–000058658

Folder label: “GCMS X 3/6/02 A 3/30/02

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Scanned page image, NYC-WTC_000058656
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

' Data File, : C:\HPCHEM\1\DATA\MAR3OO2\4941.D Vial: 8 Acq On : 29 Mar 2002 9:53 pm Operator: Sample : gc/ms scan 3/6 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\I\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************** Peak Number 1 Cyclopentasiloxane, decamethyl Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

14.84 1.86 ug/1 295708 Naphthalene-d8 15.88

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 CyclopentasiZoxane, decamethyl- 370 C10H3005Si5 000541-02-6 ^3/? 2 Benzeneeth^amine, N-[(pentafluorop 475 C21H26F5NO2Si2 055429-85-1 38 3 Phenethyla/ine, N-methyl-.beta.,3,4 399 C18H37NO3Si3 010538-85-9 32 4 Benzoic apid, 2-[(trimethylsilyl)ox 282 C13H22O3Si2 003789-85-3 28 Abunda'nee"'"'-. "... '' ..... . Sranl06704;844 mih): 494167)... .... ........ ". . 100.00% Th

5000 267 355

45 108 133 IX 177193208223 251 293 323339 [ ___ 14.60 14.80 15.00 15.20 p-m-p-TT-rj- I I ‘ ' I ' ' " 1T- ' ' I ' ' T* ] m/z 267.00 43.12% m/z-> 40 6O_.._8P_ 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #51266: Cyciopentasiloxsne, decamethyi- Th

355 267 5000 14^60 14.80 15.00 15.20 i m/z 355.05 37.11% i 191 207 251 323 339 m/z-> _ 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance Kcnzenoeiliananiine. N-Kcer-tefn.crophenyiinieib.vleno] 73 __ 14.60 14.80 15.00 15.20 5000 m/z 356.05 14.37% 267 ‘44 I 1'51 179194209 250 I

i Abundance ___ 40 60 Th 80 100 120 140 160 180 200 220 240 26C1280 300 320 340 360 #74239: Phenethyiamine, N-methyi-.beta.,3,4-tris(trimethyls l\ _____ 14.60 14.80 15.00 15.20 m/z 268.00 11.10% 5000 355 44

m/z-> X. Il 40 60 130 147 193 267 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 294 _______________________ 14.60 14.80 15.00 15.20

4941.D GCMS0308.M Tue Apr 02 11:05:30 2002 Page 1

NYC-WTC_000058656

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NYC-WTC_000058656Source: NYC Law Department, mirrored locally

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