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GCMS analysis results for sample AE12734, June 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE12679 with surrogate recovery data and identification of unknown compounds.

NYC-WTC_000015121–000015130

Folder label: “GCMS X 5/31/02 A 6/3/02

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Scanned page image, NYC-WTC_000015129
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\HPCHEM\1\DATA\JUN0302\12734 .D Vial: 12 Acq On 3 Jun 2002 8:02 pm Operator: Sample gc/ms scan 5/31 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0531.M (RTE Integrator) ... Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Anthracene-dlO- Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 25.56 0.47 ug/1 40220 Phenanthrene-dl0 25.43 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-d10- 188 C14D10 001719-06-8 86 2 Phenanthrene - dl 0 188 C14D10 001517-22-2 72 3 Naphth. lene, 1,7-dimethoxy- 188 C12H1202 005309-18-2 45 4 Antipy ine 188 C11H12N2O 000060-80-0 42 Abundance C Scan 2235 (25.564 min): 12734.D (-) m/z 188.10 100.00 188

5000

' i ■ ■ ■ ■ i ■1 ■ 1 i ■ ■ ‘ • i ■ ■ ■ ■ i ■ . 80 94 158 25.20 25.40 25.60 25.80 44 66 I .... | . I । । I ■ | n i i | i . i i 11 I i . | > |-n-> > । i i i i । . i m* . i ■ । . I Hri ri | .. ■ . | । I r m/z94.00 15.34 mlz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19957: Anthracene-d10- 1(18

5000 25.20 25.40 25.50 25.80 m/z 189.05 15.15% 160 mmH n/z—> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19958: Phenanthrene-d10 118

25.20 25.40 25.60 25.80 5000 m/z 184.10 14.93

80 94 160

mlz-> 30 m 40 50 60 66 | — । 70 80 90 100 110 120 130 140 150 160 170 180 190 i “ “ i' ■■ ■ i" ■' i ■ ■ “ i

Abundance #19913: Naphthalene, 1,7-dimethoxy- ‘ | ' I ‘ r I r-| . . . . | . . . , | . 173 11® 25.20 25.40 25.60 25.80 m/z 158.05 12.86%

5000 102 115 145

51 63 75 94 130 158 TIuTumugmmTPmTHTgus I “ i ■1" i “ ■11 ■ ■ • ■ i • I’’ miz—> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 25,20 25.40 25.60 25.80

12734.D GCMS0531.M Tue Jun 04 09:04:25 2002 Page 2

NYC-WTC_000015129

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NYC-WTC_000015129Source: NYC Law Department, mirrored locally

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