GCMS analysis results for sample AE12734, June 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\1\DATA\JUNO 302\12734.D vial: 12 Acq On 3 Jun 2002 8:02 pm Operator: Sample gc/ms scan 5/31 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0531.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 8.08 0.75 ug/1 46862 1,4-Dichlorobenzene-d4 12.07 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Pentanone, 4-hydroxy-4-methyl- 116 C6H1202 000123-42-2 78 2 1,8-Nonanediol, 8-methyl- 174 C1OH2202! 054725-73-4 9 3 2-He: nol, 2-methyl- 116 C7H160 000625-23-0 9 . 4 Prop .ne, 2-methyl-2-(1-methylethoxy 116 C7H160 017348-59-3 9 Abundance Scan 330 (8.076 min): 12734.D (-) m/z 43.00 100.00%| 43

59 5000

101 rr PaanrI? f < 7.80 8.00 8.20 8.40 83 , I ,151. II—**)****** m/z 59.00 50.67% miz-> 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #3245:2-Pentanone, 4-hydroxy-4-methyl- 43

5000 -A 59 7.80 8.00 8.20 8.40 m/z 58.0,0 19.56

mz-> 31 epsahgonigi TTHT 20 30 40 50 60 70 73.83 . 101.... 80 90 100 110 120 130 Abundance #16264:1,8-Nonanediol, 8-methyl- 50 * • i 1 * • * । AAI 7.80 8.00 8.20 8.40 5000 m/z 100.95 15.01%

69 83 miz-> 20 30 -2-4 40 50 |......... 'I1' " I60 70 98 ‘ i‘ • ■ ■ i ‘‘'i■■■ ■i•‘ 123 ‘ i ‘ 1 ■ ‘ i 1 80 90 100 110 120 130 Abundance #64354:2-Hexanol, 2-methyl- 50 7.80 8.00 8.20 8.40 m/z 40.90 9.02% 5000 43 101 69 83 ■ i ■ ' ■ ■ i 11 1 ' I ' ' ' 1 I ' MI ■ 1 1 ■ i ■ 1 ■ ■ i ■ i ■ • ‘ ■ i 1 ■ 1 1 i ' ■ ■ ■ i • ■ ■ ■ i ■ m/z—> 20 30 40 50 60 70 80 90 100 110 120 130 7.80 8.00 8.20 8.40

12734.D GCMS0531.M Tue Jun 04 09:04:25 2002 Page 1

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